REQUEST_ID|JOB_ID|SAMPLE_ID|SAMPLE_SITE|FIELD_ID|SAMPLE_DATE|SAMPLE_TIME|ANALYSIS_DATE|ANALYSIS_TIME|PARAM_CODE|PARAM_NAME|RESULT|VALUE_QUAL|UOM|MDL|PQL|PREP_METHOD|PREP_DESC|PREP_DATE|PREP_TIME|ANALYSIS_METHOD|SAMPLER|LAB_COMMENTS RQ-2017-06-26-09|TLH-2017-07-03-03|1910861|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|07-JUL-2017|06:48||Total Alkalinity|117|Y|mg CaCO3/L|0.65|2.5|||||SM 2320 B-97|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910861|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|03-JUL-2017|12:55|76|Turbidity|12|AYQ|NTU|0.10|0.10|||||EPA 180.1 Rev. 2.0|B.Paswater, K.DeAeth|The sample expired prior to receipt. Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910861|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|07-JUL-2017|03:11|951|Fluoride|1.3||mg F/L|0.18|0.50|||||SM 4500 F-C-97|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-03|1910861|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|05-JUL-2017|15:20|530|TSS|15|Y|mg/L|3.0|10|||||SM 2540 D-97|B.Paswater, K.DeAeth|Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910862|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|07-JUL-2017|07:01||Total Alkalinity|145|Y|mg CaCO3/L|0.65|2.5|||||SM 2320 B-97|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910862|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|03-JUL-2017|12:55|76|Turbidity|2.3|YQ|NTU|0.10|0.10|||||EPA 180.1 Rev. 2.0|B.Paswater, K.DeAeth|The sample expired prior to receipt. Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910862|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|07-JUL-2017|03:14|951|Fluoride|1.3||mg F/L|0.18|0.50|||||SM 4500 F-C-97|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-03|1910862|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|05-JUL-2017|15:20|530|TSS|3|IAY|mg/L|3.0|10|||||SM 2540 D-97|B.Paswater, K.DeAeth|Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910863|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|07-JUL-2017|11:54|610|Ammonia-N|0.023|Y|mg N/L|0.0020|0.0050|||||EPA 350.1 Rev. 2.0|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910863|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|11-JUL-2017|09:04|630|NO2NO3-N|0.006|IY|mg N/L|0.0040|0.010|||||EPA 353.2 Rev. 2.0|B.Paswater, K.DeAeth|NO2NO3-N: Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910863|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|10-JUL-2017|12:44|665|Total-P|0.012|YJ|mg P/L|0.0040|0.010|365.1 (MARCH 1983)|Automated, ascorbic acid|07-JUL-2017|09:45|EPA 365.1 Rev. 2.0|B.Paswater, K.DeAeth|Total-P: Sample temperature was outside the acceptable range when received at the laboratory. Refer to the narrative for an explanation of QC Codes. RQ-2017-06-26-09|TLH-2017-07-03-03|1910863|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|11-JUL-2017|15:47|625|Kjeldahl Nitrogen|0.22|IY|mg N/L|0.16|0.40|351.2 (MARCH 1983)|Preparation of samples for total kjeldahl nitrogen analysis|10-JUL-2017|13:00|EPA 351.2 Rev. 2.0|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910863|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|08-JUL-2017|10:04|680|Organic Carbon|1.9|IY|mg C/L|1.0|2.0|||||SM 5310 B-00|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910864|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|07-JUL-2017|12:00|610|Ammonia-N|0.007|Y|mg N/L|0.0020|0.0050|||||EPA 350.1 Rev. 2.0|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910864|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|11-JUL-2017|09:05|630|NO2NO3-N|0.004|UY|mg N/L|0.0040|0.010|||||EPA 353.2 Rev. 2.0|B.Paswater, K.DeAeth|NO2NO3-N: Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910864|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|10-JUL-2017|12:45|665|Total-P|0.014|Y|mg P/L|0.0040|0.010|365.1 (MARCH 1983)|Automated, ascorbic acid|07-JUL-2017|09:45|EPA 365.1 Rev. 2.0|B.Paswater, K.DeAeth|Total-P: Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910864|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|11-JUL-2017|15:49|625|Kjeldahl Nitrogen|0.47|Y|mg N/L|0.16|0.40|351.2 (MARCH 1983)|Preparation of samples for total kjeldahl nitrogen analysis|10-JUL-2017|13:00|EPA 351.2 Rev. 2.0|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910864|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|08-JUL-2017|10:20|680|Organic Carbon|3.7|Y|mg C/L|1.0|2.0|||||SM 5310 B-00|B.Paswater, K.DeAeth|Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910865|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|03-JUL-2017|15:09|671|O-Phosphate-P|0.004|UYQ|mg P/L|0.0040|0.010|||||EPA 365.1 Rev. 2.0|B.Paswater, K.DeAeth|O-Phosphate-P: The sample expired prior to receipt. Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-03|1910866|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|03-JUL-2017|15:20|671|O-Phosphate-P|0.005|IYQ|mg P/L|0.0040|0.010|||||EPA 365.1 Rev. 2.0|B.Paswater, K.DeAeth|O-Phosphate-P: The sample expired prior to receipt. Sample temperature was outside the acceptable range when received at the laboratory. RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|06-JUL-2017|18:50|1045|Iron|120|U|ug/L|120|480|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.7 Rev. 4.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|20:55|1002|Arsenic|2.2|I|ug/L|0.75|3.0|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|20:55|1027|Cadmium|0.15|U|ug/L|0.15|0.60|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|17:24|1034|Chromium|1.2|U|ug/L|1.2|4.8|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|20:55|1042|Copper|1.5|U|ug/L|1.5|3.0|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|17:24|1051|Lead|0.80|U|ug/L|0.80|3.2|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|17:24|1067|Nickel|1.0|U|ug/L|1.0|4.0|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|13-JUL-2017|17:24|1077|Silver|0.10|U|ug/L|0.10|0.40|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910869|Indian Key Fill at SW End|G5SD062917-18|29-JUN-2017|09:00|14-JUL-2017|15:55|1092|Zinc|20|U|ug/L|20|80|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|06-JUL-2017|19:01|1045|Iron|120|U|ug/L|120|480|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.7 Rev. 4.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|21:04|1002|Arsenic|2.4|I|ug/L|0.75|3.0|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|21:04|1027|Cadmium|0.15|U|ug/L|0.15|0.60|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|17:33|1034|Chromium|1.2|U|ug/L|1.2|4.8|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|21:04|1042|Copper|1.5|U|ug/L|1.5|3.0|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|17:33|1051|Lead|0.80|U|ug/L|0.80|3.2|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|17:33|1067|Nickel|1.0|U|ug/L|1.0|4.0|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|13-JUL-2017|17:33|1077|Silver|0.10|U|ug/L|0.10|0.40|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth| RQ-2017-06-26-09|TLH-2017-07-03-05|1910870|Grassey Key @ Curry Hammock SP Creek|G5SD062917-21|29-JUN-2017|08:00|14-JUL-2017|16:00|1092|Zinc|20|U|ug/L|20|80|200.2|Sample prep procedure for spectrochemical determination of total recoverable elements|03-JUL-2017|12:45|EPA 200.8 Rev. 5.4|B.Paswater, K.DeAeth|