REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 Total Alkalinity 101 0.65 mg CaCO3/L 2.5 03-21-2019 02:54 SM 2320 B-97 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 76 Turbidity 19 0.10 NTU 0.13 03-12-2019 16:50 EPA 180.1 Rev. 2.0 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 940 Chloride 16 0.20 mg Cl/L 0.60 03-21-2019 00:22 EPA 300.0 Rev. 2.1 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 80 Color (true) 17 A 2.5 PCU 6.0 03-12-2019 16:28 SM 2120 B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 951 Fluoride 0.11 0.035 mg F/L 0.10 03-21-2019 02:54 SM 4500 F-C-97 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 945 Sulfate 45 0.20 mg SO4/L 0.60 Sulfate: Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 03-20-2019 02:08 EPA 300.0 Rev. 2.1 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 70300 TDS 200 15 mg/L 25 03-13-2019 14:03 SM 2540 C-97 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068861 530 TSS 3 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 03-13-2019 14:03 SM 2540 D-97 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068862 610 Ammonia-N 0.12 0.0020 mg N/L 0.0050 03-15-2019 12:09 EPA 350.1 Rev. 2.0 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068862 630 NO2NO3-N 0.18 0.0040 mg N/L 0.010 03-15-2019 10:15 EPA 353.2 Rev. 2.0 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068862 665 Total-P 0.057 0.0050 mg P/L 0.050 03-15-2019 14:20 03-18-2019 10:06 EPA 365.1 Rev. 2.0 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068862 625 Kjeldahl Nitrogen 0.47 0.080 mg N/L 0.20 03-14-2019 12:00 03-15-2019 12:23 EPA 351.2 Rev. 2.0 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068862 680 Organic Carbon 5.9 0.50 mg C/L 1.0 03-18-2019 11:40 SM 5310 B-00 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068863 671 O-Phosphate-P 0.026 0.0040 mg P/L 0.010 03-12-2019 15:32 EPA 365.1 Rev. 2.0 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 99937 Sucralose 0.23 0.010 ug/L 0.040 03-12-2019 15:00 03-13-2019 01:45 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 AMPA 0.10 U 0.10 ug/L 0.40 03-12-2019 15:00 03-12-2019 17:37 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Acesulfame K 0.35 I 0.10 ug/L 0.40 03-12-2019 15:00 03-13-2019 01:45 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Endothall 0.25 U 0.25 ug/L 1.0 03-12-2019 15:00 03-13-2019 01:45 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Glufosinate 0.10 U 0.10 ug/L 0.40 03-12-2019 15:00 03-12-2019 17:37 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Glyphosate 0.10 U 0.10 ug/L 0.40 03-12-2019 15:00 03-12-2019 17:37 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Acetaminophen 0.020 I 0.0080 ug/L 0.032 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Bentazon 0.016 8.0E-04 ug/L 0.0032 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Carbamazepine 0.0012 I 8.0E-04 ug/L 0.0032 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Diuron 0.0020 U 0.0020 ug/L 0.0080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Fenuron 0.016 U 0.016 ug/L 0.064 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Ibuprofen 0.020 U 0.020 ug/L 0.080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Imazapyr 0.052 0.0040 ug/L 0.016 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Imidacloprid 0.0092 0.0020 ug/L 0.0080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Linuron 0.0040 U 0.0040 ug/L 0.016 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 MCPP 0.0027 I 0.0020 ug/L 0.0080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Naproxen 0.0080 U 0.0080 ug/L 0.032 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Primidone 0.0051 I 0.0040 ug/L 0.016 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068881 Triclopyr 0.0040 U 0.0040 ug/L 0.016 03-13-2019 10:00 03-16-2019 08:01 EPA 8321B C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1007 Barium 56.7 1.0 ug/L 4.0 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 916 Calcium 43.5 0.075 mg/L 0.30 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1045 Iron 2.39E+03 30 ug/L 120 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 927 Magnesium 7.93 0.040 mg/L 0.16 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 937 Potassium 2.5 0.30 mg/L 1.2 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 929 Sodium 13.3 0.50 mg/L 2.0 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1092 Zinc 6.5 I 5.0 ug/L 20 03-13-2019 17:35 03-14-2019 14:59 EPA 200.7 Rev. 4.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1105 Aluminum 58 5.0 ug/L 20 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1097 Antimony 0.13 I 0.050 ug/L 0.20 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1002 Arsenic 1.19 0.050 ug/L 0.20 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1022 Boron 48.4 2.0 ug/L 8.0 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1027 Cadmium 0.020 U 0.020 ug/L 0.080 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1034 Chromium 0.49 I 0.40 ug/L 1.6 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1042 Copper 0.67 I 0.40 ug/L 0.80 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1051 Lead 0.31 I 0.20 ug/L 0.40 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1067 Nickel 0.53 I 0.50 ug/L 2.0 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1147 Selenium 0.27 I 0.20 ug/L 0.80 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1077 Silver 0.010 U 0.010 ug/L 0.040 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068882 1059 Thallium 0.10 U 0.10 ug/L 0.40 03-13-2019 17:35 03-16-2019 09:38 EPA 200.8 Rev. 5.4 C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Acetochlor 0.27 U 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Alachlor 0.27 U 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 82184 Ametryn 0.64 U 0.64 ng/L 2.6 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39033 Atrazine 0.44 I 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Atrazine Desethyl 1.6 U 1.6 ng/L 6.4 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Azinphos Methyl 5.4 UJ 5.4 ng/L 21 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Bromacil 180 2.7 ng/L 11 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-21-2019 18:15 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Butylate 0.43 U 0.43 ng/L 1.7 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 38932 Chlorpyrifos Ethyl 0.27 UJ 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 38740 Chlorpyrifos Methyl 0.11 UJ 0.11 ng/L 0.43 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Cyanazine 3.5 U 3.5 ng/L 14 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Demeton 7.5 UJ 7.5 ng/L 30 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Diazinon 0.13 UJ 0.13 ng/L 0.54 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Dimethenamid 0.11 U 0.11 ng/L 0.43 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 81888 Disulfoton 0.54 UJ 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Dithiopyr 0.11 U 0.11 ng/L 0.43 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 EPTC 1.3 U 1.3 ng/L 5.4 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39398 Ethion 0.16 UJ 0.16 ng/L 0.64 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 81758 Ethoprop 0.11 UJ 0.11 ng/L 0.43 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Fenamiphos 0.54 UJ 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Fipronil 1.1 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Fipronil Desulfinyl 0.13 U 0.13 ng/L 0.54 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Fipronil Sulfide 2.6 0.16 ng/L 0.64 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Fipronil Sulfone 2.9 0.16 ng/L 0.64 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Fonofos 0.21 UJ 0.21 ng/L 0.86 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 38815 Hexazinone 20 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39530 Malathion 0.38 UJ 0.38 ng/L 1.5 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Metalaxyl 0.32 U 0.32 ng/L 1.3 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Metolachlor 0.54 U 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 81408 Metribuzin 0.80 U 0.80 ng/L 3.2 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39610 Mevinphos 0.54 UJ 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Molinate 0.32 U 0.32 ng/L 1.3 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 78064 Norflurazon 0.54 U 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Oxadiazon 0.31 I 0.11 ng/L 0.43 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Parathion Ethyl 0.27 UJ 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Parathion Methyl 0.59 UJ 0.59 ng/L 2.4 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Pendimethalin 1.1 U 1.1 ng/L 4.3 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 46313 Phorate 0.27 UJ 0.27 ng/L 1.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Prodiamine 0.19 UJ 0.19 ng/L 0.75 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39056 Prometon 1.8 I 0.97 ng/L 3.8 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39057 Prometryn 0.21 U 0.21 ng/L 0.86 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 39055 Simazine 0.54 U 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Tebuconazole 0.54 UJ 0.54 ng/L 2.1 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 82088 Terbufos 0.11 UJ 0.11 ng/L 0.43 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish RQ-2019-03-04-17 LONG BR @ LIBERTY ST JAX G2NE0165 G2NE0165 03-11-2019 09:50 2068883 Terbuthylazine 0.46 U 0.46 ng/L 1.8 MS accuracies for atrazine, metalaxyl, oxidiazon, fipronil sulfide, fipronil sulfone, and fipronil not assessed due to high content of these parameters in the sample spiked. Refer to the narrative for an explanation of QC Codes. Some reported results are J qualified due to surrogate recovery exceeding control limits; the sample was re-extracted and re-analyzed beyond expiration with acceptable surrogate recovery and the same analytical results were obtained. 03-18-2019 09:08 03-20-2019 15:24 EPA 8270D C.Ruben / J.Parrish