REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 Total Alkalinity 1.7 I 0.65 mg CaCO3/L 2.5 07-26-2019 05:00 SM 2320 B-97 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 76 Turbidity 3.5 0.10 NTU 0.13 07-24-2019 17:04 EPA 180.1 Rev. 2.0 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 940 Chloride 5.8 0.20 mg Cl/L 0.60 07-25-2019 15:32 EPA 300.0 Rev. 2.1 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 80 Color (true) 430 10 PCU 24 07-24-2019 18:08 SM 2120 B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 951 Fluoride 0.13 0.035 mg F/L 0.10 Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample. 07-26-2019 05:00 SM 4500 F-C-97 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 945 Sulfate 2.1 0.20 mg SO4/L 0.60 07-25-2019 15:32 EPA 300.0 Rev. 2.1 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 70300 TDS 140 15 mg/L 25 07-25-2019 13:30 SM 2540 C-97 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105365 530 TSS 4 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-25-2019 13:30 SM 2540 D-97 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105366 610 Ammonia-N 0.015 0.0020 mg N/L 0.0050 08-06-2019 16:18 EPA 350.1 Rev. 2.0 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105366 630 NO2NO3-N 0.007 I 0.0040 mg N/L 0.010 07-26-2019 09:33 EPA 353.2 Rev. 2.0 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105366 665 Total-P 0.29 0.0050 mg P/L 0.050 07-25-2019 12:40 07-26-2019 11:13 EPA 365.1 Rev. 2.0 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105366 625 Kjeldahl Nitrogen 1.2 0.080 mg N/L 0.20 Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample. 07-26-2019 13:00 07-29-2019 14:44 EPA 351.2 Rev. 2.0 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105366 680 Organic Carbon 44 0.50 mg C/L 1.0 07-25-2019 20:54 SM 5310 B-00 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105367 671 O-Phosphate-P 0.24 0.0040 mg P/L 0.010 07-24-2019 16:43 EPA 365.1 Rev. 2.0 B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 99937 Sucralose 0.010 U 0.010 ug/L 0.040 07-25-2019 11:00 08-06-2019 13:48 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 AMPA 0.10 U 0.10 ug/L 0.40 07-25-2019 11:00 07-29-2019 11:47 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Acesulfame K 0.10 U 0.10 ug/L 0.40 07-25-2019 11:00 07-27-2019 22:00 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Endothall 0.25 U 0.25 ug/L 1.0 07-25-2019 11:00 07-27-2019 22:00 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Glufosinate 0.10 U 0.10 ug/L 0.40 07-25-2019 11:00 07-29-2019 11:47 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Glyphosate 0.10 U 0.10 ug/L 0.40 07-25-2019 11:00 07-29-2019 11:47 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Acetamiprid 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Bentazon 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Clothianidin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Dinotefuran 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Diuron 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Imazapyr 0.025 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Imidacloprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Thiamethoxam 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Tolfenpyrad 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben RQ-2019-07-22-07 Little Creek at US 441 21010033 21010033 07-23-2019 09:55 2105371 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 07-25-2019 10:00 07-26-2019 07:32 EPA 8321B B. Davis, C. Ruben