REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106950 Total Alkalinity 97 0.65 mg CaCO3/L 2.5 08-07-2019 06:24 SM 2320 B-97 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106950 76 Turbidity 4.8 0.10 NTU 0.13 07-30-2019 17:05 EPA 180.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106950 71870 Bromide 24 1.3 mg Br/L 4.0 08-02-2019 08:25 EPA 300.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106950 951 Fluoride 0.47 0.070 mg F/L 0.20 08-10-2019 05:05 SM 4500 F-C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106950 530 TSS 6 IA 3.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-30-2019 16:50 SM 2540 D-97 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106951 610 Ammonia-N 0.014 0.0020 mg N/L 0.0050 08-08-2019 12:35 EPA 350.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106951 630 NO2NO3-N 0.018 0.0040 mg N/L 0.010 08-01-2019 09:49 EPA 353.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106951 665 Total-P 0.096 0.0040 mg P/L 0.010 07-31-2019 12:24 08-01-2019 12:04 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106951 625 Kjeldahl Nitrogen 0.66 0.16 mg N/L 0.40 08-02-2019 12:30 08-05-2019 14:20 EPA 351.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106951 680 Organic Carbon 8.5 1.0 mg C/L 2.0 08-02-2019 01:52 SM 5310 B-00 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106952 671 O-Phosphate-P 0.053 0.0040 mg P/L 0.010 07-30-2019 17:29 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 Total Alkalinity 92 0.65 mg CaCO3/L 2.5 08-06-2019 21:01 SM 2320 B-97 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 76 Turbidity 9.7 0.10 NTU 0.13 07-30-2019 17:05 EPA 180.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 940 Chloride 4.1E+03 8.0 mg Cl/L 24 08-02-2019 12:22 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 80 Color (true) 53 2.5 PCU 6.0 07-30-2019 17:53 SM 2120 B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 951 Fluoride 0.32 0.070 mg F/L 0.20 08-06-2019 17:17 SM 4500 F-C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 945 Sulfate 600 8.0 mg SO4/L 24 Sulfate: Batch matrix spike recoveries for one of two spiked samples are unavailable because of high analyte concentration in the QC sample. 08-02-2019 12:22 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 70300 TDS 7.92E+03 150 mg/L 250 07-31-2019 17:30 SM 2540 C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106953 530 TSS 18 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-31-2019 16:50 SM 2540 D-97 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106954 610 Ammonia-N 0.073 0.0020 mg N/L 0.0050 08-08-2019 12:37 EPA 350.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106954 630 NO2NO3-N 0.032 0.0040 mg N/L 0.010 08-01-2019 09:50 EPA 353.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106954 665 Total-P 0.084 0.0040 mg P/L 0.010 07-31-2019 12:24 08-01-2019 12:05 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106954 625 Kjeldahl Nitrogen 0.90 0.16 mg N/L 0.40 08-02-2019 12:30 08-05-2019 14:21 EPA 351.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106954 680 Organic Carbon 12 0.50 mg C/L 1.0 07-31-2019 23:55 SM 5310 B-00 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106955 671 O-Phosphate-P 0.026 0.0040 mg P/L 0.010 07-30-2019 17:37 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 Total Alkalinity 54 0.65 mg CaCO3/L 2.5 08-06-2019 07:47 SM 2320 B-97 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 76 Turbidity 3.9 0.10 NTU 0.13 07-30-2019 17:05 EPA 180.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 940 Chloride 35 A 0.20 mg Cl/L 0.60 08-02-2019 11:09 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 80 Color (true) 79 2.5 PCU 6.0 07-30-2019 17:54 SM 2120 B J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 951 Fluoride 0.068 I 0.035 mg F/L 0.10 08-06-2019 07:47 SM 4500 F-C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 945 Sulfate 77 A 0.20 mg SO4/L 0.60 Sulfate: Batch matrix spike recoveries for one of two spiked samples are unavailable because of high analyte concentration in the QC sample. 08-02-2019 11:09 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 70300 TDS 282 15 mg/L 25 07-31-2019 17:30 SM 2540 C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106956 530 TSS 8 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-31-2019 16:50 SM 2540 D-97 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106957 610 Ammonia-N 0.017 0.0020 mg N/L 0.0050 08-08-2019 13:28 EPA 350.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106957 630 NO2NO3-N 0.088 0.0040 mg N/L 0.010 07-31-2019 10:29 EPA 353.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106957 665 Total-P 0.060 0.0050 mg P/L 0.050 07-31-2019 12:24 08-01-2019 12:01 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106957 625 Kjeldahl Nitrogen 0.63 0.080 mg N/L 0.20 08-01-2019 18:00 08-02-2019 17:32 EPA 351.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106957 680 Organic Carbon 13 0.50 mg C/L 1.0 08-01-2019 00:07 SM 5310 B-00 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106958 671 O-Phosphate-P 0.030 0.0040 mg P/L 0.010 07-30-2019 17:41 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 Total Alkalinity 84 0.65 mg CaCO3/L 2.5 08-06-2019 08:00 SM 2320 B-97 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 76 Turbidity 3.6 0.10 NTU 0.13 07-30-2019 17:05 EPA 180.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 940 Chloride 45 0.20 mg Cl/L 0.60 08-02-2019 12:34 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 80 Color (true) 33 2.5 PCU 6.0 07-30-2019 17:58 SM 2120 B J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 951 Fluoride 0.057 I 0.035 mg F/L 0.10 08-06-2019 08:00 SM 4500 F-C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 945 Sulfate 29 0.20 mg SO4/L 0.60 Sulfate: Batch matrix spike recoveries for one of two spiked samples are unavailable because of high analyte concentration in the QC sample. 08-02-2019 12:34 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 70300 TDS 230 A 15 mg/L 25 07-31-2019 17:30 SM 2540 C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106959 530 TSS 2 IA 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-31-2019 16:50 SM 2540 D-97 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 Total Alkalinity 37 0.65 mg CaCO3/L 2.5 08-06-2019 08:13 SM 2320 B-97 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 76 Turbidity 1.9 0.10 NTU 0.13 07-30-2019 17:05 EPA 180.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 940 Chloride 33 0.20 mg Cl/L 0.60 08-02-2019 13:11 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 80 Color (true) 13 2.5 PCU 6.0 07-30-2019 17:58 SM 2120 B J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 951 Fluoride 0.035 U 0.035 mg F/L 0.10 08-06-2019 08:13 SM 4500 F-C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 945 Sulfate 30 0.20 mg SO4/L 0.60 Sulfate: Batch matrix spike recoveries for one of two spiked samples are unavailable because of high analyte concentration in the QC sample. 08-02-2019 13:11 EPA 300.0 Rev. 2.1 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 70300 TDS 147 15 mg/L 25 07-31-2019 17:30 SM 2540 C-97 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106960 530 TSS 2 U 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-31-2019 16:50 SM 2540 D-97 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106961 610 Ammonia-N 0.066 0.0020 mg N/L 0.0050 08-08-2019 13:16 EPA 350.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106961 630 NO2NO3-N 0.49 0.0040 mg N/L 0.010 07-31-2019 10:30 EPA 353.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106961 665 Total-P 0.050 0.0050 mg P/L 0.050 07-31-2019 12:24 08-01-2019 11:54 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106961 625 Kjeldahl Nitrogen 0.58 0.080 mg N/L 0.20 08-01-2019 18:00 08-02-2019 17:34 EPA 351.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106961 680 Organic Carbon 6.8 0.50 mg C/L 1.0 08-01-2019 00:21 SM 5310 B-00 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106962 610 Ammonia-N 0.093 0.0020 mg N/L 0.0050 08-08-2019 13:29 EPA 350.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106962 630 NO2NO3-N 0.26 0.0040 mg N/L 0.010 07-31-2019 10:40 EPA 353.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106962 665 Total-P 0.030 0.0020 mg P/L 0.0050 07-31-2019 12:24 08-01-2019 12:38 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106962 625 Kjeldahl Nitrogen 0.35 0.080 mg N/L 0.20 08-01-2019 18:00 08-02-2019 17:35 EPA 351.2 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106962 680 Organic Carbon 2.5 0.50 mg C/L 1.0 08-01-2019 00:36 SM 5310 B-00 J.Parrish / K.Appleby RQ-2019-07-29-12 STRAWBERRY CR AT END OF BOWLAN RD 20030579 20030579 07-29-2019 10:35 2106963 671 O-Phosphate-P 0.032 0.0040 mg P/L 0.010 07-30-2019 17:39 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 NEWCASTLE CR @ FT CAROLINE HILLS RD 20030872 20030872 07-29-2019 11:10 2106964 671 O-Phosphate-P 0.018 0.0040 mg P/L 0.010 07-30-2019 16:50 EPA 365.1 Rev. 2.0 J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 99937 Sucralose 0.68 0.010 ug/L 0.040 07-31-2019 10:15 08-12-2019 16:05 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 AMPA 1.0 U 1.0 ug/L 4.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 08-01-2019 13:58 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Acesulfame K 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 07-31-2019 16:59 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Endothall 0.25 UJ 0.25 ug/L 1.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 07-31-2019 16:59 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Glufosinate 1.0 U 1.0 ug/L 4.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 08-01-2019 13:58 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Glyphosate 1.0 U 1.0 ug/L 4.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 08-01-2019 13:58 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 39730 2,4-D 0.0083 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Bentazon 0.0087 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Carbamazepine 0.0013 I 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Diuron 0.020 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Fluridone 0.0034 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Imazapyr 0.036 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Imidacloprid 0.012 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 MCPP 0.0024 IJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 MILLER CREEK AT ATLANTIC BLVD G2NE0005 G2NE0005 07-29-2019 10:10 2106992 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 10:43 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 99937 Sucralose 0.74 0.010 ug/L 0.040 07-31-2019 10:15 08-12-2019 16:16 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 AMPA 1.0 U 1.0 ug/L 4.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 08-01-2019 14:08 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Acesulfame K 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 07-31-2019 17:13 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Endothall 0.25 UJ 0.25 ug/L 1.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 07-31-2019 17:13 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Glufosinate 1.0 U 1.0 ug/L 4.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 08-01-2019 14:08 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Glyphosate 1.5 I 1.0 ug/L 4.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. MDL for some parameters elevated due to matrix interference. 07-31-2019 10:15 08-01-2019 14:08 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 39730 2,4-D 0.63 0.040 ug/L 0.16 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-06-2019 00:40 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Bentazon 0.037 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Clothianidin 0.033 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Dinotefuran 0.0029 I 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Diuron 0.0095 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Fluridone 1.1 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-06-2019 00:40 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Imazapyr 1.4 0.080 ug/L 0.32 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-06-2019 00:40 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Imidacloprid 0.073 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 MCPP 0.0079 IJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106993 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for acetaminophen and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. Refer to the narrative for an explanation of QC Codes. 08-01-2019 10:00 08-02-2019 11:18 EPA 8321B J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1007 Barium 33.2 1.0 ug/L 4.0 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 21:55 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 916 Calcium 122 0.075 mg/L 0.30 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 21:55 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1045 Iron 400 30 ug/L 120 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 21:55 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 927 Magnesium 294 0.80 mg/L 3.2 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 22:03 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1055 Manganese 41.6 1.0 ug/L 4.0 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 21:55 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 937 Potassium 98 6.0 mg/L 24 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 22:03 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 929 Sodium 2.58E+03 10 mg/L 40 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 22:03 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1092 Zinc 5.0 U 5.0 ug/L 20 Batch matrix spike recoveries for calcium, magnesium, potassium and sodium are unavailable because of high analyte concentration in the QC sample. 07-31-2019 15:35 08-01-2019 21:55 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1105 Aluminum 276 20 ug/L 80 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1097 Antimony 0.21 I 0.20 ug/L 0.80 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1002 Arsenic 2.17 0.20 ug/L 0.80 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1022 Boron 997 8.0 ug/L 32 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1027 Cadmium 0.080 U 0.080 ug/L 0.32 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1034 Chromium 4.0 U 4.0 ug/L 16 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-16-2019 21:22 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1042 Copper 3.3 1.6 ug/L 3.2 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1051 Lead 0.80 U 0.80 ug/L 1.6 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1067 Nickel 2.0 U 2.0 ug/L 8.0 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1147 Selenium 2.0 U 2.0 ug/L 8.0 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-21-2019 01:08 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1077 Silver 0.040 U 0.040 ug/L 0.16 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 GREENFIELD CREEK @ QUEENS HARBOUR BLVD 20030809 20030809 07-29-2019 11:55 2106994 1059 Thallium 0.40 U 0.40 ug/L 1.6 Batch matrix spike recoveries for boron are unavailable because of high analyte concentration in the QC sample. The sample required dilution due to matrix interference. 07-31-2019 15:35 08-17-2019 03:34 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1007 Barium 34.3 1.0 ug/L 4.0 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 916 Calcium 44.7 0.075 mg/L 0.30 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1045 Iron 240 30 ug/L 120 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 927 Magnesium 10.1 0.040 mg/L 0.16 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 937 Potassium 2.5 0.30 mg/L 1.2 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 929 Sodium 20.0 0.50 mg/L 2.0 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1092 Zinc 5.0 U 5.0 ug/L 20 07-31-2019 18:00 08-02-2019 15:48 EPA 200.7 Rev. 4.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1105 Aluminum 183 5.0 ug/L 20 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1097 Antimony 0.078 I 0.050 ug/L 0.20 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1002 Arsenic 0.78 0.050 ug/L 0.20 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1022 Boron 31.7 2.0 ug/L 8.0 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1027 Cadmium 0.020 U 0.020 ug/L 0.080 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1034 Chromium 0.40 U 0.40 ug/L 1.6 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1042 Copper 3.00 0.40 ug/L 0.80 07-31-2019 18:00 08-21-2019 21:44 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1051 Lead 0.20 U 0.20 ug/L 0.40 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1067 Nickel 0.88 I 0.50 ug/L 2.0 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1147 Selenium 0.20 U 0.20 ug/L 0.80 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1077 Silver 0.010 U 0.010 ug/L 0.040 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby RQ-2019-07-29-12 PUNCHEON ABOVE POINT MEADOWS DR G2NE1181 G2NE1181 07-29-2019 12:30 2106995 1059 Thallium 0.10 U 0.10 ug/L 0.40 07-31-2019 18:00 08-09-2019 02:25 EPA 200.8 Rev. 5.4 J.Parrish / K.Appleby