REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 Total Alkalinity 8.1 0.65 mg CaCO3/L 2.5 08-23-2019 09:51 SM 2320 B-97 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 76 Turbidity 1.3 0.10 NTU 0.13 08-16-2019 16:33 EPA 180.1 Rev. 2.0 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 940 Chloride 6.5 0.20 mg Cl/L 0.60 08-22-2019 10:40 EPA 300.0 Rev. 2.1 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 80 Color (true) 710 18 PCU 42 08-16-2019 17:25 SM 2120 B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 951 Fluoride 0.14 0.035 mg F/L 0.10 08-23-2019 09:51 SM 4500 F-C-97 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 945 Sulfate 0.83 0.20 mg SO4/L 0.60 Sulfate: Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-22-2019 10:40 EPA 300.0 Rev. 2.1 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 70300 TDS 156 15 mg/L 25 The result was confirmed on 08/28/2019. 08-21-2019 14:21 SM 2540 C-97 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112416 530 TSS 2 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-21-2019 14:21 SM 2540 D-97 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112417 610 Ammonia-N 0.036 0.0020 mg N/L 0.0050 08-27-2019 11:19 EPA 350.1 Rev. 2.0 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112417 630 NO2NO3-N 0.026 0.0040 mg N/L 0.010 08-21-2019 11:38 EPA 353.2 Rev. 2.0 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112417 665 Total-P 0.31 0.0050 mg P/L 0.050 08-20-2019 12:45 08-21-2019 12:09 EPA 365.1 Rev. 2.0 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112417 625 Kjeldahl Nitrogen 1.4 0.080 mg N/L 0.20 08-21-2019 13:20 08-22-2019 15:24 EPA 351.2 Rev. 2.0 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112417 680 Organic Carbon 60 0.50 mg C/L 1.0 08-21-2019 03:05 SM 5310 B-00 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112418 671 O-Phosphate-P 0.25 0.0040 mg P/L 0.010 08-16-2019 12:10 EPA 365.1 Rev. 2.0 JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 99937 Sucralose 0.010 U 0.010 ug/L 0.040 08-21-2019 10:00 08-28-2019 12:12 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 AMPA 0.10 U 0.10 ug/L 0.40 08-21-2019 10:00 08-21-2019 19:19 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Acesulfame K 0.10 U 0.10 ug/L 0.40 08-21-2019 10:00 08-21-2019 11:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Endothall 0.25 U 0.25 ug/L 1.0 08-21-2019 10:00 08-21-2019 11:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Glufosinate 0.10 U 0.10 ug/L 0.40 08-21-2019 10:00 08-21-2019 19:19 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Glyphosate 0.10 U 0.10 ug/L 0.40 08-21-2019 10:00 08-21-2019 19:19 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Bentazon 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Diuron 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Imazapyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Imidacloprid 0.0025 I 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER RQ-2019-08-05-22 LITTLE CREEK AT US 441 21010033 21010033 08-15-2019 09:55 2112422 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for bentazon, dinotefuran and imazapyr could not be assessed due to high concentration of parameter in the spiked sample. 08-22-2019 09:00 08-24-2019 08:59 EPA 8321B JEREMY PARRISH/AMY KALMBACHER