REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109771 Total Alkalinity 170 0.65 mg CaCO3/L 2.5 08-15-2019 14:28 SM 2320 B-97 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109771 76 Turbidity 7.1 0.10 NTU 0.13 08-08-2019 17:07 EPA 180.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109771 71870 Bromide 0.65 0.13 mg Br/L 0.40 08-20-2019 01:08 EPA 300.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109771 951 Fluoride 0.48 0.035 mg F/L 0.10 08-15-2019 14:28 SM 4500 F-C-97 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109771 530 TSS 2 UA 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-09-2019 15:30 SM 2540 D-97 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109772 610 Ammonia-N 0.35 0.020 mg N/L 0.050 08-15-2019 13:56 EPA 350.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109772 630 NO2NO3-N 0.40 0.0040 mg N/L 0.010 08-13-2019 13:07 EPA 353.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109772 665 Total-P 0.13 0.0050 mg P/L 0.050 08-12-2019 13:21 08-13-2019 11:48 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109772 625 Kjeldahl Nitrogen 0.70 J 0.080 mg N/L 0.20 Refer to the narrative for an explanation of QC Codes. 08-13-2019 12:36 08-14-2019 12:08 EPA 351.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109772 680 Organic Carbon 5.1 0.50 mg C/L 1.0 08-09-2019 21:41 SM 5310 B-00 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109773 671 O-Phosphate-P 0.048 0.0040 mg P/L 0.010 08-08-2019 15:07 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109774 Total Alkalinity O 0.0 mg CaCO3/L 0.0 Insufficent sample volume to perform the analysis. 08-15-2019 19:28 SM 2320 B-97 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109774 76 Turbidity 7.1 0.10 NTU 0.13 08-08-2019 17:07 EPA 180.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109774 71870 Bromide 22 0.65 mg Br/L 2.0 08-20-2019 01:59 EPA 300.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109774 951 Fluoride O 0.0 mg F/L 0.0 Insufficent sample volume to perform the analysis. 08-15-2019 19:28 SM 4500 F-C-97 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109774 530 TSS 13 3.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-13-2019 15:51 SM 2540 D-97 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109775 Total Alkalinity 97 0.65 mg CaCO3/L 2.5 08-16-2019 07:11 SM 2320 B-97 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109775 76 Turbidity 7.0 0.10 NTU 0.13 08-08-2019 17:07 EPA 180.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109775 71870 Bromide 35 1.3 mg Br/L 4.0 08-20-2019 02:17 EPA 300.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109775 951 Fluoride 0.68 0.18 mg F/L 0.50 08-16-2019 03:17 SM 4500 F-C-97 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109775 530 TSS 13 3.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-13-2019 15:51 SM 2540 D-97 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109776 Total Alkalinity 107 0.65 mg CaCO3/L 2.5 08-16-2019 07:23 SM 2320 B-97 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109776 76 Turbidity 7.7 0.10 NTU 0.13 08-08-2019 17:07 EPA 180.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109776 71870 Bromide 49 2.6 mg Br/L 8.0 08-20-2019 02:34 EPA 300.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109776 951 Fluoride 0.92 0.18 mg F/L 0.50 08-16-2019 03:21 SM 4500 F-C-97 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109776 530 TSS 13 3.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-13-2019 15:51 SM 2540 D-97 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109777 610 Ammonia-N 0.024 0.0020 mg N/L 0.0050 08-14-2019 13:29 EPA 350.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109777 630 NO2NO3-N 0.011 0.0040 mg N/L 0.010 08-12-2019 12:20 EPA 353.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109777 665 Total-P 0.11 0.0040 mg P/L 0.010 08-12-2019 13:21 08-13-2019 11:44 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109777 625 Kjeldahl Nitrogen 0.81 0.16 mg N/L 0.40 08-13-2019 14:20 08-14-2019 10:54 EPA 351.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109777 680 Organic Carbon 9.5 1.0 mg C/L 2.0 08-13-2019 23:27 SM 5310 B-00 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109778 610 Ammonia-N 0.014 0.0020 mg N/L 0.0050 08-14-2019 13:31 EPA 350.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109778 630 NO2NO3-N 0.038 0.0040 mg N/L 0.010 08-12-2019 12:21 EPA 353.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109778 665 Total-P 0.091 0.0040 mg P/L 0.010 08-12-2019 13:21 08-13-2019 11:45 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109778 625 Kjeldahl Nitrogen 0.73 0.16 mg N/L 0.40 08-13-2019 14:20 08-14-2019 10:56 EPA 351.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109778 680 Organic Carbon 7.4 1.0 mg C/L 2.0 08-13-2019 23:39 SM 5310 B-00 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109779 610 Ammonia-N 0.032 0.0020 mg N/L 0.0050 08-14-2019 13:32 EPA 350.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109779 630 NO2NO3-N 0.024 0.0040 mg N/L 0.010 08-12-2019 12:22 EPA 353.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109779 665 Total-P 0.077 0.0040 mg P/L 0.010 08-12-2019 13:21 08-13-2019 11:46 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109779 625 Kjeldahl Nitrogen 0.68 0.16 mg N/L 0.40 08-13-2019 14:20 08-14-2019 11:28 EPA 351.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109779 680 Organic Carbon 5.7 1.0 mg C/L 2.0 08-13-2019 23:51 SM 5310 B-00 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109780 671 O-Phosphate-P 0.066 0.0040 mg P/L 0.010 08-08-2019 14:58 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109781 671 O-Phosphate-P 0.066 0.0040 mg P/L 0.010 08-08-2019 14:58 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109782 671 O-Phosphate-P 0.044 0.0040 mg P/L 0.010 08-08-2019 14:59 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109783 Total Alkalinity 100 0.65 mg CaCO3/L 2.5 08-16-2019 07:35 SM 2320 B-97 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109783 76 Turbidity 5.8 0.10 NTU 0.13 08-08-2019 17:07 EPA 180.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109783 71870 Bromide 42 2.6 mg Br/L 8.0 08-20-2019 02:51 EPA 300.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109783 951 Fluoride 0.81 0.18 mg F/L 0.50 08-16-2019 03:25 SM 4500 F-C-97 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109783 530 TSS 10 3.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-13-2019 15:51 SM 2540 D-97 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109784 610 Ammonia-N 0.014 0.0020 mg N/L 0.0050 08-14-2019 13:34 EPA 350.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109784 630 NO2NO3-N 0.019 0.0040 mg N/L 0.010 08-12-2019 12:23 EPA 353.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109784 665 Total-P 0.067 0.0040 mg P/L 0.010 08-12-2019 13:21 08-13-2019 11:47 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109784 625 Kjeldahl Nitrogen 0.65 0.16 mg N/L 0.40 08-13-2019 14:20 08-14-2019 11:30 EPA 351.2 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109784 680 Organic Carbon 6.7 1.0 mg C/L 2.0 08-14-2019 20:22 SM 5310 B-00 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109785 671 O-Phosphate-P 0.030 0.0040 mg P/L 0.010 08-08-2019 14:33 EPA 365.1 Rev. 2.0 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 99937 Sucralose 0.12 0.010 ug/L 0.040 08-08-2019 15:30 08-19-2019 21:23 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 AMPA 0.41 0.10 ug/L 0.40 08-08-2019 15:30 08-13-2019 20:03 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Acesulfame K 0.10 U 0.10 ug/L 0.40 08-08-2019 15:30 08-13-2019 13:51 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Endothall 0.25 U 0.25 ug/L 1.0 08-08-2019 15:30 08-13-2019 13:51 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Glufosinate 0.10 U 0.10 ug/L 0.40 08-08-2019 15:30 08-13-2019 20:03 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Glyphosate 0.32 I 0.10 ug/L 0.40 08-08-2019 15:30 08-13-2019 20:03 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 39730 2,4-D 0.0085 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Bentazon 0.0014 I 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Diuron 0.013 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Imazapyr 0.22 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Imidacloprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Thiamethoxam 0.0023 I 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109798 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 11:54 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 99937 Sucralose 0.27 0.010 ug/L 0.040 08-08-2019 15:30 08-19-2019 21:46 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 AMPA 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-08-2019 15:30 08-13-2019 20:24 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Acesulfame K 0.10 U 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-08-2019 15:30 08-13-2019 14:21 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Endothall 0.25 U 0.25 ug/L 1.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-08-2019 15:30 08-13-2019 14:21 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Glufosinate 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-08-2019 15:30 08-13-2019 20:24 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Glyphosate 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-08-2019 15:30 08-13-2019 20:24 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 39730 2,4-D 0.0085 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Bentazon 0.0075 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Diuron 0.0082 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Fluridone 0.048 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Imazapyr 0.068 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Imidacloprid 0.0097 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 MCPP 0.0024 I 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109799 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imazapyr could not be assessed due to high concentration of parameter in the spiked sample. MS accuracy and precision for bentazon could not be assessed due to high concentration of parameter in the spiked sample. 08-12-2019 10:00 08-14-2019 12:29 EPA 8321B C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1045 Iron 940 30 ug/L 120 08-12-2019 14:45 08-13-2019 15:25 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1055 Manganese 124 1.0 ug/L 4.0 08-12-2019 14:45 08-13-2019 15:25 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1092 Zinc 5.0 U 5.0 ug/L 20 08-12-2019 14:45 08-13-2019 15:25 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1105 Aluminum 54 5.0 ug/L 20 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1097 Antimony 0.13 I 0.050 ug/L 0.20 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1002 Arsenic 6.59 0.050 ug/L 0.20 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1027 Cadmium 0.020 U 0.020 ug/L 0.080 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1034 Chromium 0.60 I 0.40 ug/L 1.6 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1042 Copper 0.73 I 0.40 ug/L 0.80 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1051 Lead 0.98 0.20 ug/L 0.40 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1067 Nickel 0.50 U 0.50 ug/L 2.0 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1147 Selenium 0.20 U 0.20 ug/L 0.80 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1077 Silver 0.010 U 0.010 ug/L 0.040 08-12-2019 14:45 08-23-2019 07:19 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DEER CR @ TALLEYRAND AVE 20030792 20030792 08-07-2019 11:15 2109812 1059 Thallium 0.10 U 0.10 ug/L 0.40 08-12-2019 14:45 08-28-2019 05:38 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1045 Iron 350 I 90 ug/L 360 08-14-2019 16:15 08-15-2019 15:56 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1055 Manganese 39 3.0 ug/L 12 08-14-2019 16:15 08-15-2019 15:56 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1092 Zinc 15 U 15 ug/L 60 08-14-2019 16:15 08-15-2019 15:56 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1105 Aluminum 310 50 ug/L 200 08-14-2019 16:15 09-05-2019 02:59 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1097 Antimony 0.50 U 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 02:59 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1002 Arsenic 2.6 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 02:59 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1027 Cadmium 0.20 U 0.20 ug/L 0.80 08-14-2019 16:15 09-05-2019 02:59 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1034 Chromium 4.0 U 4.0 ug/L 16 08-14-2019 16:15 09-06-2019 17:52 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1042 Copper 1.6 U 1.6 ug/L 3.2 08-14-2019 16:15 09-06-2019 19:18 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1051 Lead 2.0 U 2.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 02:59 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1067 Nickel 5.0 U 5.0 ug/L 20 08-14-2019 16:15 09-06-2019 17:52 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1147 Selenium 2.0 U 2.0 ug/L 8.0 08-14-2019 16:15 09-05-2019 02:59 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1077 Silver 0.10 U 0.10 ug/L 0.40 08-14-2019 16:15 09-06-2019 17:52 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 DUNN CR AT FAYE ROAD 20030140 20030140 08-07-2019 09:20 2109813 1059 Thallium 1.0 U 1.0 ug/L 4.0 08-14-2019 16:15 09-09-2019 18:41 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1045 Iron 300 I 90 ug/L 360 08-14-2019 16:15 08-15-2019 16:49 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1055 Manganese 13 3.0 ug/L 12 08-14-2019 16:15 08-15-2019 16:49 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1092 Zinc 15 U 15 ug/L 60 08-14-2019 16:15 08-15-2019 16:49 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1105 Aluminum 360 50 ug/L 200 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1097 Antimony 0.50 U 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1002 Arsenic 2.6 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1027 Cadmium 0.20 U 0.20 ug/L 0.80 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1034 Chromium 4.0 U 4.0 ug/L 16 08-14-2019 16:15 09-09-2019 05:52 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1042 Copper 1.8 I 1.6 ug/L 3.2 08-14-2019 16:15 09-09-2019 07:13 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1051 Lead 2.0 U 2.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1067 Nickel 5.0 U 5.0 ug/L 20 08-14-2019 16:15 09-09-2019 05:52 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1147 Selenium 2.0 U 2.0 ug/L 8.0 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1077 Silver 0.10 U 0.10 ug/L 0.40 08-14-2019 16:15 09-06-2019 18:11 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 St. Johns River at Ft. Caroline dock G2NE1179 G2NE1179 08-07-2019 10:00 2109814 1059 Thallium 1.0 U 1.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 03:27 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1045 Iron 310 I 90 ug/L 360 08-14-2019 16:15 08-15-2019 16:57 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1055 Manganese 15 3.0 ug/L 12 08-14-2019 16:15 08-15-2019 16:57 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1092 Zinc 15 U 15 ug/L 60 08-14-2019 16:15 08-15-2019 16:57 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1105 Aluminum 440 50 ug/L 200 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1097 Antimony 0.50 U 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1002 Arsenic 2.9 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1027 Cadmium 0.20 U 0.20 ug/L 0.80 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1034 Chromium 4.0 U 4.0 ug/L 16 08-14-2019 16:15 09-09-2019 06:00 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1042 Copper 1.6 U 1.6 ug/L 3.2 08-14-2019 16:15 09-09-2019 07:21 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1051 Lead 2.0 U 2.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1067 Nickel 5.0 U 5.0 ug/L 20 08-14-2019 16:15 09-09-2019 06:00 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1147 Selenium 2.0 U 2.0 ug/L 8.0 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1077 Silver 0.10 U 0.10 ug/L 0.40 08-14-2019 16:15 09-06-2019 18:17 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 SISTERS CREEK AT HECKSCHER DR 20030491 20030491 08-07-2019 08:45 2109815 1059 Thallium 1.0 U 1.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 03:37 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1045 Iron 180 I 90 ug/L 360 08-14-2019 16:15 08-15-2019 17:04 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1055 Manganese 21 3.0 ug/L 12 08-14-2019 16:15 08-15-2019 17:04 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1092 Zinc 15 U 15 ug/L 60 08-14-2019 16:15 08-15-2019 17:04 EPA 200.7 Rev. 4.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1105 Aluminum 310 50 ug/L 200 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1097 Antimony 0.50 U 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1002 Arsenic 3.1 0.50 ug/L 2.0 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1027 Cadmium 0.20 U 0.20 ug/L 0.80 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1034 Chromium 4.0 U 4.0 ug/L 16 08-14-2019 16:15 09-09-2019 06:08 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1042 Copper 1.6 U 1.6 ug/L 3.2 08-14-2019 16:15 09-09-2019 07:29 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1051 Lead 2.0 U 2.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1067 Nickel 5.0 U 5.0 ug/L 20 08-14-2019 16:15 09-09-2019 06:08 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1147 Selenium 2.0 U 2.0 ug/L 8.0 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1077 Silver 0.10 U 0.10 ug/L 0.40 08-14-2019 16:15 09-06-2019 18:23 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby RQ-2019-08-05-33 Greenfield end of Bucaneer dr. G2NE1154 G2NE1154 08-07-2019 10:30 2109816 1059 Thallium 1.0 U 1.0 ug/L 4.0 08-14-2019 16:15 09-05-2019 03:46 EPA 200.8 Rev. 5.4 C. Ruben, K. Appleby