REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 Total Alkalinity 6.2 0.65 mg CaCO3/L 2.5 08-23-2019 02:38 SM 2320 B-97 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 76 Turbidity 3.8 0.10 NTU 0.13 08-15-2019 16:59 EPA 180.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 940 Chloride 12 0.20 mg Cl/L 0.60 08-22-2019 00:45 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 80 Color (true) 470 12 PCU 30 08-15-2019 16:38 SM 2120 B C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 951 Fluoride 0.041 I 0.035 mg F/L 0.10 08-23-2019 02:38 SM 4500 F-C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 945 Sulfate 1.7 0.20 mg SO4/L 0.60 08-22-2019 00:45 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 70300 TDS 97 15 mg/L 25 08-16-2019 17:15 SM 2540 C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112030 530 TSS 4 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-16-2019 17:15 SM 2540 D-97 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 Total Alkalinity 31 0.65 mg CaCO3/L 2.5 08-23-2019 02:51 SM 2320 B-97 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 76 Turbidity 5.4 A 0.10 NTU 0.13 08-15-2019 16:59 EPA 180.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 940 Chloride 13 0.20 mg Cl/L 0.60 08-22-2019 00:58 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 80 Color (true) 370 10 PCU 24 08-15-2019 16:51 SM 2120 B C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 951 Fluoride 0.088 I 0.035 mg F/L 0.10 08-23-2019 02:51 SM 4500 F-C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 945 Sulfate 27 0.20 mg SO4/L 0.60 08-22-2019 00:58 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 70300 TDS 164 A 15 mg/L 25 08-16-2019 17:15 SM 2540 C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112031 530 TSS 4 IA 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-16-2019 17:15 SM 2540 D-97 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112032 610 Ammonia-N 0.028 0.0020 mg N/L 0.0050 08-26-2019 12:57 EPA 350.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112032 630 NO2NO3-N 0.004 U 0.0040 mg N/L 0.010 08-21-2019 10:24 EPA 353.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112032 665 Total-P 0.032 0.0020 mg P/L 0.0050 08-20-2019 12:45 08-21-2019 12:46 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112032 625 Kjeldahl Nitrogen 1.2 0.080 mg N/L 0.20 08-21-2019 13:20 08-22-2019 12:20 EPA 351.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112032 680 Organic Carbon 38 0.50 mg C/L 1.0 08-20-2019 01:14 SM 5310 B-00 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112033 610 Ammonia-N 0.074 0.0020 mg N/L 0.0050 08-26-2019 12:59 EPA 350.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112033 630 NO2NO3-N 0.027 0.0040 mg N/L 0.010 08-21-2019 10:26 EPA 353.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112033 665 Total-P 0.30 0.0050 mg P/L 0.050 08-20-2019 12:45 08-21-2019 11:13 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112033 625 Kjeldahl Nitrogen 1.5 0.080 mg N/L 0.20 08-21-2019 13:20 08-22-2019 12:22 EPA 351.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112033 680 Organic Carbon 36 0.50 mg C/L 1.0 08-20-2019 01:51 SM 5310 B-00 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112034 671 O-Phosphate-P 0.006 I 0.0040 mg P/L 0.010 08-15-2019 14:56 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112035 671 O-Phosphate-P 0.21 0.0040 mg P/L 0.010 08-15-2019 14:55 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 Total Alkalinity 39 0.65 mg CaCO3/L 2.5 08-23-2019 03:50 SM 2320 B-97 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 76 Turbidity 3.2 0.10 NTU 0.13 08-15-2019 16:59 EPA 180.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 940 Chloride 610 2.0 mg Cl/L 6.0 08-22-2019 01:10 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 80 Color (true) 160 5.0 PCU 12 08-15-2019 16:39 SM 2120 B C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 951 Fluoride 0.092 I 0.035 mg F/L 0.10 08-23-2019 03:50 SM 4500 F-C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 945 Sulfate 79 2.0 mg SO4/L 6.0 08-22-2019 01:10 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 70300 TDS 1.27E+03 30 mg/L 50 08-16-2019 17:15 SM 2540 C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112036 530 TSS 4 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-16-2019 17:15 SM 2540 D-97 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 Total Alkalinity 5.9 0.65 mg CaCO3/L 2.5 08-23-2019 03:02 SM 2320 B-97 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 76 Turbidity 4.4 0.10 NTU 0.13 08-15-2019 16:59 EPA 180.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 940 Chloride 12 0.20 mg Cl/L 0.60 08-22-2019 01:22 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 80 Color (true) 190 5.0 PCU 12 08-15-2019 16:52 SM 2120 B C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 951 Fluoride 0.035 U 0.035 mg F/L 0.10 08-23-2019 03:02 SM 4500 F-C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 945 Sulfate 4.1 0.20 mg SO4/L 0.60 08-22-2019 01:22 EPA 300.0 Rev. 2.1 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 70300 TDS 68 15 mg/L 25 08-16-2019 17:15 SM 2540 C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112037 530 TSS 2 U 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-16-2019 17:15 SM 2540 D-97 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112038 610 Ammonia-N 0.005 0.0020 mg N/L 0.0050 08-26-2019 13:15 EPA 350.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112038 630 NO2NO3-N 0.004 I 0.0040 mg N/L 0.010 08-21-2019 10:27 EPA 353.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112038 665 Total-P 0.077 0.0050 mg P/L 0.050 08-20-2019 12:45 08-21-2019 11:14 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112038 625 Kjeldahl Nitrogen 0.80 0.080 mg N/L 0.20 08-21-2019 13:20 08-22-2019 12:24 EPA 351.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112038 680 Organic Carbon 20 0.50 mg C/L 1.0 08-19-2019 20:05 SM 5310 B-00 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112039 610 Ammonia-N 0.005 0.0020 mg N/L 0.0050 08-26-2019 13:18 EPA 350.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112039 630 NO2NO3-N 0.004 U 0.0040 mg N/L 0.010 08-21-2019 10:28 EPA 353.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112039 665 Total-P 0.025 0.0020 mg P/L 0.0050 08-20-2019 12:45 08-21-2019 12:47 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112039 625 Kjeldahl Nitrogen 0.55 0.080 mg N/L 0.20 08-21-2019 13:20 08-22-2019 12:28 EPA 351.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112039 680 Organic Carbon 17 0.50 mg C/L 1.0 08-20-2019 05:28 SM 5310 B-00 C. Ruben, B. Paris RQ-2019-08-12-16 Lofton CR @ A1A 19020003 19020003 08-14-2019 12:40 2112040 671 O-Phosphate-P 0.037 0.0040 mg P/L 0.010 08-15-2019 14:57 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Creek draining former Hampton Lake 100m above Rd. G4NE0292 G4NE0292 08-14-2019 10:30 2112041 671 O-Phosphate-P 0.007 I 0.0040 mg P/L 0.010 08-15-2019 14:28 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112042 Total Alkalinity 135 0.65 mg CaCO3/L 2.5 08-27-2019 00:05 SM 2320 B-97 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112042 76 Turbidity 12 A 0.10 NTU 0.13 08-15-2019 16:59 EPA 180.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112042 71870 Bromide 71 2.6 mg Br/L 8.0 08-20-2019 20:31 EPA 300.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112042 951 Fluoride 1.2 0.18 mg F/L 0.50 08-26-2019 21:58 SM 4500 F-C-97 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112042 530 TSS 22 3.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 08-19-2019 15:20 SM 2540 D-97 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112043 610 Ammonia-N 0.044 0.0020 mg N/L 0.0050 08-26-2019 12:04 EPA 350.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112043 630 NO2NO3-N 0.008 I 0.0040 mg N/L 0.010 08-23-2019 10:35 EPA 353.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112043 665 Total-P 0.10 0.0040 mg P/L 0.010 08-20-2019 12:45 08-21-2019 12:34 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112043 625 Kjeldahl Nitrogen 0.74 0.16 mg N/L 0.40 08-22-2019 11:15 08-23-2019 10:51 EPA 351.2 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112043 680 Organic Carbon 6.2 1.0 mg C/L 2.0 08-20-2019 03:29 SM 5310 B-00 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112044 671 O-Phosphate-P 0.055 0.0040 mg P/L 0.010 08-15-2019 14:43 EPA 365.1 Rev. 2.0 C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 99937 Sucralose 0.010 U 0.010 ug/L 0.040 08-15-2019 14:45 08-28-2019 09:51 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 AMPA 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-15-2019 14:45 08-19-2019 11:53 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Acesulfame K 0.10 U 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-15-2019 14:45 08-16-2019 17:56 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Endothall 0.25 U 0.25 ug/L 1.0 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-15-2019 14:45 08-16-2019 17:56 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Glufosinate 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-15-2019 14:45 08-19-2019 11:53 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Glyphosate 0.10 UJ 0.10 ug/L 0.40 Refer to the narrative for an explanation of QC Codes. Surrogate spike recovery exceeding the control limits. Results confirmed in sample duplicate. 08-15-2019 14:45 08-19-2019 11:53 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Bentazon 0.0036 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Diuron 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Imazapyr 0.024 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Imidacloprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Tolfenpyrad 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Egans Creek at N. 14th G4NE0290 G4NE0290 08-14-2019 13:15 2112056 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for imidacloprid could not be assessed due to high concentration of parameter in the spiked sample. Matrix spike precision for tolfenpyad is not available due to low analyte recoveries. Refer to the narrative for an explanation of QC Codes. 08-16-2019 09:30 08-18-2019 11:57 EPA 8321B C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1007 Barium 25.5 1.0 ug/L 4.0 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 916 Calcium 5.97 0.075 mg/L 0.30 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1045 Iron 2.52E+03 30 ug/L 120 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 927 Magnesium 1.81 0.040 mg/L 0.16 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 937 Potassium 1.3 0.30 mg/L 1.2 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 929 Sodium 8.4 0.50 mg/L 2.0 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1092 Zinc 5.0 U 5.0 ug/L 20 08-20-2019 16:10 08-21-2019 16:17 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1105 Aluminum 548 5.0 ug/L 20 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1097 Antimony 0.050 U 0.050 ug/L 0.20 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1002 Arsenic 0.94 0.050 ug/L 0.20 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1022 Boron 25.0 2.0 ug/L 8.0 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1027 Cadmium 0.020 U 0.020 ug/L 0.080 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1034 Chromium 0.77 I 0.40 ug/L 1.6 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1042 Copper 0.40 U 0.40 ug/L 0.80 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1051 Lead 0.79 0.20 ug/L 0.40 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1067 Nickel 0.78 I 0.50 ug/L 2.0 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-07-2019 00:39 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1147 Selenium 0.20 U 0.20 ug/L 0.80 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1077 Silver 0.010 U 0.010 ug/L 0.040 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-07-2019 00:39 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Mills Creek at US 301/US1 19020048 19020048 08-14-2019 11:20 2112057 1059 Thallium 0.10 U 0.10 ug/L 0.40 The lead result was confirmed in the undigested sample on 09/11/2019. 08-20-2019 16:10 09-04-2019 21:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1007 Barium 33.4 1.0 ug/L 4.0 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 916 Calcium 19.3 0.075 mg/L 0.30 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1045 Iron 1.29E+03 30 ug/L 120 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 927 Magnesium 6.00 0.040 mg/L 0.16 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 937 Potassium 4.7 0.30 mg/L 1.2 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 929 Sodium 10.5 0.50 mg/L 2.0 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1092 Zinc 11 I 5.0 ug/L 20 08-20-2019 16:10 08-21-2019 16:23 EPA 200.7 Rev. 4.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1105 Aluminum 442 5.0 ug/L 20 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1097 Antimony 0.11 I 0.050 ug/L 0.20 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1002 Arsenic 1.56 0.050 ug/L 0.20 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1022 Boron 39.8 2.0 ug/L 8.0 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1027 Cadmium 0.020 U 0.020 ug/L 0.080 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1034 Chromium 0.96 I 0.40 ug/L 1.6 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1042 Copper 2.08 0.40 ug/L 0.80 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1051 Lead 0.51 0.20 ug/L 0.40 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1067 Nickel 1.2 I 0.50 ug/L 2.0 08-20-2019 16:10 09-07-2019 00:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1147 Selenium 0.28 I 0.20 ug/L 0.80 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1077 Silver 0.010 U 0.010 ug/L 0.040 08-20-2019 16:10 09-07-2019 00:45 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris RQ-2019-08-12-16 Unnamed Branch above Alligator CR. G4NE0288 G4NE0288 08-14-2019 09:20 2112058 1059 Thallium 0.10 U 0.10 ug/L 0.40 08-20-2019 16:10 09-04-2019 21:54 EPA 200.8 Rev. 5.4 C. Ruben, B. Paris