REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 Total Alkalinity 51 0.65 mg CaCO3/L 2.5 11-08-2019 12:03 SM 2320 B-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 76 Turbidity 1.0 A 0.10 NTU 0.13 10-30-2019 15:14 EPA 180.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 940 Chloride 5.1 0.20 mg Cl/L 0.60 11-05-2019 16:15 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 80 Color (true) 83 2.5 PCU 6.0 10-30-2019 14:34 SM 2120 B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 951 Fluoride 0.28 0.035 mg F/L 0.10 11-01-2019 10:08 SM 4500 F-C-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 945 Sulfate 1.8 0.20 mg SO4/L 0.60 11-05-2019 16:15 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 70300 TDS 84 15 mg/L 25 11-01-2019 14:21 SM 2540 C-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132356 530 TSS 2 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 11-01-2019 14:21 SM 2540 D-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 Total Alkalinity 51 0.65 mg CaCO3/L 2.5 11-08-2019 12:12 SM 2320 B-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 76 Turbidity 1.2 0.10 NTU 0.13 10-30-2019 15:14 EPA 180.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 940 Chloride 5.1 0.20 mg Cl/L 0.60 11-05-2019 16:27 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 80 Color (true) 83 2.5 PCU 6.0 10-30-2019 14:35 SM 2120 B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 951 Fluoride 0.27 0.035 mg F/L 0.10 11-01-2019 10:38 SM 4500 F-C-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 945 Sulfate 1.6 0.20 mg SO4/L 0.60 11-05-2019 16:27 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 70300 TDS 77 15 mg/L 25 11-01-2019 14:21 SM 2540 C-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132357 530 TSS 2 U 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 11-01-2019 14:21 SM 2540 D-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132358 610 Ammonia-N 0.006 0.0020 mg N/L 0.0050 11-01-2019 12:05 EPA 350.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132358 630 NO2NO3-N 0.007 I 0.0040 mg N/L 0.010 10-31-2019 09:59 EPA 353.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132358 665 Total-P 0.54 0.0050 mg P/L 0.050 Total-P: Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample 10-31-2019 12:13 11-01-2019 16:00 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132358 625 Kjeldahl Nitrogen 0.30 0.080 mg N/L 0.20 11-06-2019 12:31 11-08-2019 14:55 EPA 351.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132358 680 Organic Carbon 7.6 0.50 mg C/L 1.0 10-31-2019 19:01 SM 5310 B-00 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132359 610 Ammonia-N 0.006 0.0020 mg N/L 0.0050 11-01-2019 12:07 EPA 350.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132359 630 NO2NO3-N 0.007 I 0.0040 mg N/L 0.010 10-31-2019 10:00 EPA 353.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132359 665 Total-P 0.55 0.0050 mg P/L 0.050 Total-P: Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample 10-31-2019 12:13 11-01-2019 16:04 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132359 625 Kjeldahl Nitrogen 0.30 0.080 mg N/L 0.20 11-06-2019 12:31 11-08-2019 14:57 EPA 351.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132359 680 Organic Carbon 7.6 0.50 mg C/L 1.0 10-31-2019 19:16 SM 5310 B-00 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132360 671 O-Phosphate-P 0.48 0.040 mg P/L 0.10 10-30-2019 18:16 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132361 671 O-Phosphate-P 0.49 0.040 mg P/L 0.10 10-30-2019 18:17 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 Total Alkalinity 7.8 0.65 mg CaCO3/L 2.5 11-08-2019 12:21 SM 2320 B-97 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 76 Turbidity 2.4 0.10 NTU 0.13 10-30-2019 15:14 EPA 180.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 940 Chloride 7.6 0.20 mg Cl/L 0.60 11-05-2019 16:39 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 80 Color (true) 56 A 2.5 PCU 6.0 10-30-2019 14:36 SM 2120 B J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 951 Fluoride 0.12 0.035 mg F/L 0.10 11-01-2019 11:07 SM 4500 F-C-97 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 945 Sulfate 3.8 0.20 mg SO4/L 0.60 11-05-2019 16:39 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 70300 TDS 36 15 mg/L 25 11-01-2019 14:21 SM 2540 C-97 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132362 530 TSS 4 I 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 11-01-2019 14:21 SM 2540 D-97 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132363 610 Ammonia-N 0.057 0.0020 mg N/L 0.0050 11-01-2019 12:08 EPA 350.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132363 630 NO2NO3-N 0.012 0.0040 mg N/L 0.010 10-31-2019 10:01 EPA 353.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132363 665 Total-P 0.17 0.0050 mg P/L 0.050 Total-P: Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample 10-31-2019 12:13 11-01-2019 16:05 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132363 625 Kjeldahl Nitrogen 0.72 0.080 mg N/L 0.20 11-06-2019 12:31 11-08-2019 14:58 EPA 351.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132363 680 Organic Carbon 8.7 0.50 mg C/L 1.0 10-31-2019 20:00 SM 5310 B-00 J. Parrish RQ-2019-10-28-09 Peacock Lake Center 21020097 21020097 10-29-2019 10:10 2132364 671 O-Phosphate-P 0.075 0.0040 mg P/L 0.010 10-30-2019 18:19 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 Total Alkalinity 0.65 U 0.65 mg CaCO3/L 2.5 11-08-2019 12:28 SM 2320 B-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 76 Turbidity 0.10 U 0.10 NTU 0.13 10-30-2019 15:14 EPA 180.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 940 Chloride 0.20 U 0.20 mg Cl/L 0.60 11-05-2019 16:51 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 80 Color (true) 2.5 U 2.5 PCU 6.0 10-30-2019 14:37 SM 2120 B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 951 Fluoride 0.035 U 0.035 mg F/L 0.10 11-01-2019 12:46 SM 4500 F-C-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 945 Sulfate 0.20 U 0.20 mg SO4/L 0.60 11-05-2019 16:51 EPA 300.0 Rev. 2.1 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 70300 TDS 15 U 15 mg/L 25 11-01-2019 14:21 SM 2540 C-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132365 530 TSS 2 U 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 11-01-2019 14:21 SM 2540 D-97 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132366 610 Ammonia-N 0.002 U 0.0020 mg N/L 0.0050 11-01-2019 12:32 EPA 350.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132366 630 NO2NO3-N 0.004 U 0.0040 mg N/L 0.010 10-31-2019 10:02 EPA 353.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132366 665 Total-P 0.002 U 0.0020 mg P/L 0.0050 Total-P: Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample. 10-31-2019 12:13 11-01-2019 16:31 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132366 625 Kjeldahl Nitrogen 0.080 U 0.080 mg N/L 0.20 11-06-2019 12:31 11-08-2019 15:00 EPA 351.2 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132366 680 Organic Carbon 0.50 U 0.50 mg C/L 1.0 10-31-2019 20:15 SM 5310 B-00 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132367 671 O-Phosphate-P 0.004 U 0.0040 mg P/L 0.010 10-30-2019 17:49 EPA 365.1 Rev. 2.0 J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 99937 Sucralose 0.010 I 0.010 ug/L 0.040 10-31-2019 11:30 11-13-2019 17:21 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 AMPA 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:34 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Acesulfame K 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 10-31-2019 19:13 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Endothall 0.25 U 0.25 ug/L 1.0 10-31-2019 11:30 10-31-2019 19:13 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Glufosinate 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:34 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Glyphosate 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:34 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Bentazon 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Diuron 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Imazapyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Imidacloprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033 21010033 10-29-2019 11:30 2132375 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:18 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 99937 Sucralose 0.012 I 0.010 ug/L 0.040 10-31-2019 11:30 11-13-2019 17:32 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 AMPA 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:44 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Acesulfame K 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 10-31-2019 19:27 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Endothall 0.25 U 0.25 ug/L 1.0 10-31-2019 11:30 10-31-2019 19:27 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Glufosinate 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:44 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Glyphosate 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:44 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Bentazon 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Diuron 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Imazapyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Imidacloprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 21010033DUP 21010033 10-29-2019 11:35 2132376 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-11-2019 15:53 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 99937 Sucralose 0.010 U 0.010 ug/L 0.040 10-31-2019 11:30 11-13-2019 17:44 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 AMPA 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:55 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Acesulfame K 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 10-31-2019 19:41 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Endothall 0.25 U 0.25 ug/L 1.0 10-31-2019 11:30 10-31-2019 19:41 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Glufosinate 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:55 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Glyphosate 0.10 U 0.10 ug/L 0.40 10-31-2019 11:30 11-01-2019 21:55 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 39730 2,4-D 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Acetaminophen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Acetamiprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Afidopyropen 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Bentazon 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Benzovindiflupyr 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Carbamazepine 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Clothianidin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Dinotefuran 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Diuron 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Fenuron 0.016 U 0.016 ug/L 0.064 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Fluridone 8.0E-04 U 8.0E-04 ug/L 0.0032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Hydrocodone 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Ibuprofen 0.020 U 0.020 ug/L 0.080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Imazapyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Imidacloprid 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Linuron 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 MCPP 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Mandestrobin 0.0020 UJ 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Naproxen 0.0080 U 0.0080 ug/L 0.032 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Primidone 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Pyraclostrobin 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Thiamethoxam 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Tolfenpyrad 0.0020 U 0.0020 ug/L 0.0080 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish RQ-2019-10-28-09 Little Creek at US 441 SMPFB102919 10-29-2019 11:45 2132377 Triclopyr 0.0040 U 0.0040 ug/L 0.016 J - second source check standards for some analytes were not available for analysis. MS accuracy for some analytes could not be assessed due to high concentration of parameter in the spiked sample. 11-01-2019 10:30 11-09-2019 00:33 EPA 8321B J. Parrish