REQUEST_ID|JOB_ID|SAMPLE_ID|SAMPLE_SITE|FIELD_ID|SAMPLE_DATE|SAMPLE_TIME|ANALYSIS_DATE|ANALYSIS_TIME|PARAM_CODE|PARAM_NAME|RESULT|VALUE_QUAL|UOM|MDL|PQL|PREP_METHOD|PREP_DESC|PREP_DATE|PREP_TIME|ANALYSIS_METHOD|SAMPLER|LAB_COMMENTS RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|07-SEP-2021|19:37||Total Alkalinity|22||mg CaCO3/L|0.65|2.5|||||SM 2320 B-2011|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|02-SEP-2021|13:29|76|Turbidity|2.6||NTU|0.10|0.13|||||EPA 180.1 Rev. 2.0|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|08-SEP-2021|16:07|940|Chloride|25||mg Cl/L|0.20|0.50|||||EPA 300.0 Rev. 2.1|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|02-SEP-2021|15:18|80|Color (true)|360||PCU|7.5|18|||||SM 2120 B-2011|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|07-SEP-2021|19:37|951|Fluoride|0.077|I|mg F/L|0.035|0.10|||||SM 4500 F-C-2011|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|08-SEP-2021|16:07|945|Sulfate|9.0||mg SO4/L|0.20|0.50|||||EPA 300.0 Rev. 2.1|William Mullen, Monica Jeager|Sulfate: Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|03-SEP-2021|14:31|70300|TDS|143||mg/L|15|25|||||SM 2540 C-2011|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273241|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|03-SEP-2021|14:31|530|TSS|4|I|mg/L|2.0|10|||||SM 2540 D-2011|William Mullen, Monica Jeager|Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. RQ-2021-09-06-68|TLH-2021-09-02-29|2273242|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|03-SEP-2021|13:22|610|Ammonia-N|0.020||mg N/L|0.0020|0.0050|||||EPA 350.1 Rev. 2.0|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273242|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|03-SEP-2021|09:21|630|NO2NO3-N|0.050||mg N/L|0.0040|0.010|||||EPA 353.2 Rev. 2.0|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273242|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|08-SEP-2021|10:29|665|Total-P|0.14||mg P/L|0.0050|0.050|365.1 (MARCH 1983)|Automated, ascorbic acid|07-SEP-2021|15:50|EPA 365.1 Rev. 2.0|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273242|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|10-SEP-2021|11:26|625|Kjeldahl Nitrogen|1.5||mg N/L|0.080|0.20|351.2 (MARCH 1983)|Preparation of samples for total kjeldahl nitrogen analysis|09-SEP-2021|12:30|EPA 351.2 Rev. 2.0|William Mullen, Monica Jeager|Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample. RQ-2021-09-06-68|TLH-2021-09-02-29|2273242|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|09-SEP-2021|02:48|680|Organic Carbon|35||mg C/L|0.50|1.0|||||SM 5310 B-2011|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-29|2273243|Bee Branch @ Loblolly Bay Rd.|G3SD0085|01-SEP-2021|09:05|02-SEP-2021|16:38|671|O-Phosphate-P|0.096||mg P/L|0.0040|0.010|||||EPA 365.1 Rev. 2.0|William Mullen, Monica Jeager| RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|03-SEP-2021|10:57||AMPA|0.78||ug/L|0.10|0.40|LC-FILTER|Filtration of samples prior to analysis|03-SEP-2021|08:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for Glyphosate could not be assessed due to a high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|03-SEP-2021|13:21||Acesulfame K|0.22|I|ug/L|0.10|0.40|LC-FILTER|Filtration of samples prior to analysis|03-SEP-2021|08:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for Glyphosate could not be assessed due to a high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|03-SEP-2021|13:21||Endothall|0.25|U|ug/L|0.25|1.0|LC-FILTER|Filtration of samples prior to analysis|03-SEP-2021|08:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for Glyphosate could not be assessed due to a high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|03-SEP-2021|10:57||Glufosinate|0.10|U|ug/L|0.10|0.40|LC-FILTER|Filtration of samples prior to analysis|03-SEP-2021|08:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for Glyphosate could not be assessed due to a high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|03-SEP-2021|10:57||Glyphosate|3.1||ug/L|0.10|0.40|LC-FILTER|Filtration of samples prior to analysis|03-SEP-2021|08:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for Glyphosate could not be assessed due to a high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|03-SEP-2021|13:21||Sucralose|0.13||ug/L|0.010|0.040|LC-FILTER|Filtration of samples prior to analysis|03-SEP-2021|08:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for Glyphosate could not be assessed due to a high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23|39740|2,4,5-T|0.0040|U|ug/L|0.0040|0.016|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23|39730|2,4-D|0.037||ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Acetaminophen|0.017|I|ug/L|0.0080|0.032|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Acetamiprid|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Afidopyropen|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Bentazon|0.0044||ug/L|8.0E-04|0.0032|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Benzovindiflupyr|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Carbamazepine|8.0E-04|U|ug/L|8.0E-04|0.0032|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Clothianidin|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Dinotefuran|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Diuron|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Fenuron|0.016|U|ug/L|0.016|0.064|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Fluridone|8.0E-04|U|ug/L|8.0E-04|0.0032|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Hydrocodone|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Ibuprofen|0.020|U|ug/L|0.020|0.080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Imazapyr|0.019||ug/L|0.0040|0.016|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Imidacloprid|0.013||ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Linuron|0.0040|U|ug/L|0.0040|0.016|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||MCPP|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Mandestrobin|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Naproxen|0.0080|U|ug/L|0.0080|0.032|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Primidone|0.0040|U|ug/L|0.0040|0.016|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Pyraclostrobin|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Thiamethoxam|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Tolfenpyrad|0.0020|U|ug/L|0.0020|0.0080|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample. RQ-2021-09-06-68|TLH-2021-09-02-35|2273251|Palm Creek @ Lee Civic Ctr.|G3SD0190|01-SEP-2021|08:20|08-SEP-2021|16:23||Triclopyr|0.0040|U|ug/L|0.0040|0.016|3535A|Prep for herbicides and carbamates|03-SEP-2021|14:00|EPA 8321B|William Mullen, Monica Jeager|MS accuracy for 2,4-D could not be assessed due to high concentration of parameter in the spiked sample.