REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 Total Alkalinity 138 A 0.65 mg CaCO3/L 2.5 07-06-2022 23:46 SM 2320 B-2011 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 76 Turbidity 0.10 U 0.10 NTU 1.0 07-01-2022 14:42 EPA 180.1 Rev. 2.0 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 940 Chloride 6.1 0.20 mg Cl/L 0.50 07-12-2022 03:58 EPA 300.0 Rev. 2.1 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 80 Color (true) 2.5 U 2.5 PCU 6.0 07-01-2022 14:37 DEP SOP: NU-094-1 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 951 Fluoride 0.069 I 0.035 mg F/L 0.10 07-06-2022 23:35 SM 4500-F- C-2011 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 945 Sulfate 12 0.20 mg SO4/L 0.50 07-12-2022 03:58 EPA 300.0 Rev. 2.1 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 70300 TDS 171 A 15 mg/L 25 07-05-2022 16:02 SM 2540 C-2011 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338595 530 TSS 2 UA 2.0 mg/L 10 Batch relative percent difference is unavailable because of low analyte concentration in the QC sample. 07-05-2022 16:02 SM 2540 D-2011 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338596 610 Ammonia-N 0.002 I 0.0020 mg N/L 0.0050 07-08-2022 11:08 EPA 350.1 Rev. 2.0 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338596 630 NO2NO3-N 2.0 0.020 mg N/L 0.050 07-12-2022 12:47 EPA 353.2 Rev. 2.0 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338596 665 Total-P 0.038 0.0020 mg P/L 0.0050 07-07-2022 16:00 07-11-2022 11:55 EPA 365.1 Rev. 2.0 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338596 625 Kjeldahl Nitrogen 0.10 I 0.080 mg N/L 0.20 Batch matrix spike recoveries are unavailable because of high analyte concentration in the QC sample. 07-06-2022 09:21 07-07-2022 13:58 EPA 351.2 Rev. 2.0 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Twin Spring at vent G1NE0943 G1NE0943 06-30-2022 12:05 2338596 680 Organic Carbon 0.50 U 0.50 mg C/L 1.0 07-07-2022 18:01 SM 5310 B-2011 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Chlordane 2.6 U 2.6 ng/L 13 07-07-2022 08:00 07-13-2022 12:18 EPA 8276 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Toxaphene 16 U 16 ng/L 78 07-07-2022 08:00 07-13-2022 12:18 EPA 8276 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1016 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1221 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1232 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1242 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1248 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1254 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 PCB-1260 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-09-2022 03:24 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39330 Aldrin 0.68 U 0.68 ng/L 3.4 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39337 Alpha-BHC 0.10 U 0.10 ng/L 0.52 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Alpha-Chlordane 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39338 Beta-BHC 0.10 U 0.10 ng/L 0.52 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Beta-Cyfluthrin 1.3 U 1.3 ng/L 6.5 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Bifenthrin 0.52 U 0.52 ng/L 2.6 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39786 Carbophenothion 0.94 U 0.94 ng/L 4.7 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 70314 Chlorothalonil 1.3 U 1.3 ng/L 7.8 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Cis-Nonachlor 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 3781 Cypermethrin 1.6 U 1.6 ng/L 7.8 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39310 DDD-p,p' 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39320 DDE-p,p' 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39300 DDT-p,p' 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Dacthal 0.16 U 0.16 ng/L 0.78 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 34259 Delta-BHC 0.42 U 0.42 ng/L 2.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Deltamethrin 1.3 U 1.3 ng/L 6.5 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Dichlobenil 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Dicofol 1.3 U 1.3 ng/L 6.5 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39380 Dieldrin 0.42 U 0.42 ng/L 2.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 34361 Endosulfan I 0.42 U 0.42 ng/L 2.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 34356 Endosulfan II 0.42 U 0.42 ng/L 2.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 34351 Endosulfan Sulfate 0.31 U 0.31 ng/L 1.6 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39390 Endrin 0.42 U 0.42 ng/L 2.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 34366 Endrin Aldehyde 0.78 U 0.78 ng/L 3.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Endrin Ketone 0.42 U 0.42 ng/L 2.1 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Esfenvalerate 0.78 U 0.78 ng/L 3.9 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Ethalfluralin 0.16 U 0.16 ng/L 0.78 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Fenpropathrin 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39340 Gamma-BHC 0.13 U 0.13 ng/L 0.65 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Gamma-Chlordane 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39410 Heptachlor 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39420 Heptachlor Epoxide 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Hexachlorobenzene 1.0 U 1.0 ng/L 5.2 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Kepone 5.2 U 5.2 ng/L 26 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Lambda-Cyhalothrin 0.78 U 0.78 ng/L 3.9 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 MGK-264 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Methoprene 0.78 U 0.78 ng/L 3.9 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39480 Methoxychlor 0.31 U 0.31 ng/L 1.6 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 39755 Mirex 0.73 U 0.73 ng/L 3.6 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Oxychlordane 0.31 U 0.31 ng/L 1.6 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 79191 Permethrin 1.7 U 1.7 ng/L 8.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Phenothrin 0.94 U 0.94 ng/L 4.7 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Piperonyl Butoxide 0.16 U 0.16 ng/L 0.78 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Prallethrin 2.1 U 2.1 ng/L 10 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Tau-Fluvalinate 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Tetramethrin 0.78 U 0.78 ng/L 3.9 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Trans-Nonachlor 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 Triclosan Methyl 0.16 U 0.16 ng/L 0.78 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SR-18 21030071 21030071 06-30-2022 10:25 2338600 81284 Trifluralin 0.21 U 0.21 ng/L 1.0 07-07-2022 08:00 07-10-2022 02:42 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Chlordane 2.6 U 2.6 ng/L 13 07-07-2022 08:00 07-13-2022 13:14 EPA 8276 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Toxaphene 15 U 15 ng/L 77 07-07-2022 08:00 07-13-2022 13:14 EPA 8276 Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1016 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1221 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1232 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1242 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1248 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1254 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 PCB-1260 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-09-2022 03:54 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39330 Aldrin 0.66 U 0.66 ng/L 3.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39337 Alpha-BHC 0.10 U 0.10 ng/L 0.51 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Alpha-Chlordane 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39338 Beta-BHC 0.10 U 0.10 ng/L 0.51 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Beta-Cyfluthrin 1.3 U 1.3 ng/L 6.4 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Bifenthrin 0.51 U 0.51 ng/L 2.6 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39786 Carbophenothion 0.92 U 0.92 ng/L 4.6 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 70314 Chlorothalonil 1.3 U 1.3 ng/L 7.7 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Cis-Nonachlor 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 3781 Cypermethrin 1.5 U 1.5 ng/L 7.7 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39310 DDD-p,p' 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39320 DDE-p,p' 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39300 DDT-p,p' 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Dacthal 0.15 U 0.15 ng/L 0.77 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 34259 Delta-BHC 0.41 U 0.41 ng/L 2.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Deltamethrin 1.3 U 1.3 ng/L 6.4 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Dichlobenil 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Dicofol 1.3 U 1.3 ng/L 6.4 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39380 Dieldrin 0.41 U 0.41 ng/L 2.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 34361 Endosulfan I 0.41 U 0.41 ng/L 2.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 34356 Endosulfan II 0.41 U 0.41 ng/L 2.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 34351 Endosulfan Sulfate 0.31 U 0.31 ng/L 1.5 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39390 Endrin 0.41 U 0.41 ng/L 2.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 34366 Endrin Aldehyde 0.77 U 0.77 ng/L 3.1 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Endrin Ketone 0.41 U 0.41 ng/L 2.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Esfenvalerate 0.77 U 0.77 ng/L 3.8 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Ethalfluralin 0.15 U 0.15 ng/L 0.77 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Fenpropathrin 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39340 Gamma-BHC 0.13 U 0.13 ng/L 0.64 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Gamma-Chlordane 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39410 Heptachlor 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39420 Heptachlor Epoxide 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Hexachlorobenzene 1.0 U 1.0 ng/L 5.1 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Kepone 5.1 U 5.1 ng/L 26 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Lambda-Cyhalothrin 0.77 U 0.77 ng/L 3.8 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 MGK-264 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Methoprene 0.77 U 0.77 ng/L 3.8 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39480 Methoxychlor 0.31 U 0.31 ng/L 1.5 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 39755 Mirex 0.72 U 0.72 ng/L 3.6 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Oxychlordane 0.31 U 0.31 ng/L 1.5 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 79191 Permethrin 1.6 U 1.6 ng/L 8.2 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Phenothrin 0.92 U 0.92 ng/L 4.6 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Piperonyl Butoxide 0.60 I 0.15 ng/L 0.77 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Prallethrin 2.0 U 2.0 ng/L 10 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Tau-Fluvalinate 0.26 U 0.26 ng/L 1.3 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Tetramethrin 0.77 U 0.77 ng/L 3.8 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Trans-Nonachlor 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 Triclosan Methyl 0.15 U 0.15 ng/L 0.77 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis RQ-2022-05-16-21 Olustee Creek at SE Union Way G1NE0951 G1NE0951 06-30-2022 10:55 2338601 81284 Trifluralin 0.20 U 0.20 ng/L 1.0 07-07-2022 08:00 07-10-2022 03:11 EPA 8270E Katrin Villinger/Brian Davis