REQUEST_ID SAMPLE_SITE FIELD_ID STORET_STATION SAMPLE_DATE SAMPLE_TIME SAMPLE_ID PARAM_CODE PARAM_NAME RESULT VALUE_QUAL MDL UOM PQL LAB_COMMENTS PREP_DATE PREP_TIME ANALYSIS_DATE ANALYSIS_TIME ANALYSIS_METHOD SAMPLER RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 Total Alkalinity 21 0.65 mg CaCO3/L 2.5 06-13-2022 00:32 SM 2320 B-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 76 Turbidity 3.4 A 0.10 NTU 1.0 06-02-2022 14:16 EPA 180.1 Rev. 2.0 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 940 Chloride 17 0.20 mg Cl/L 0.50 06-08-2022 23:44 EPA 300.0 Rev. 2.1 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 80 Color (true) 210 7.5 PCU 18 06-02-2022 14:41 DEP SOP: NU-094-1 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 951 Fluoride 0.040 I 0.035 mg F/L 0.10 06-13-2022 00:32 SM 4500-F- C-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 945 Sulfate 25 0.20 mg SO4/L 0.50 06-08-2022 23:44 EPA 300.0 Rev. 2.1 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 70300 TDS 143 15 mg/L 25 06-03-2022 14:44 SM 2540 C-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331295 530 TSS 2 U 2.0 mg/L 10 06-03-2022 14:44 SM 2540 D-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331296 610 Ammonia-N 0.024 0.0020 mg N/L 0.0050 06-17-2022 15:27 EPA 350.1 Rev. 2.0 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331296 630 NO2NO3-N 0.014 0.0040 mg N/L 0.010 06-14-2022 18:15 EPA 353.2 Rev. 2.0 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331296 665 Total-P 0.031 0.0020 mg P/L 0.0050 06-06-2022 15:34 06-07-2022 14:26 EPA 365.1 Rev. 2.0 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331296 625 Kjeldahl Nitrogen 0.84 0.080 mg N/L 0.20 06-08-2022 09:10 06-10-2022 14:42 EPA 351.2 Rev. 2.0 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331296 680 Organic Carbon 24 0.50 mg C/L 1.0 06-04-2022 01:12 SM 5310 B-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 46570 Hardness 52.8 0.35 mg/L 1.4 06-08-2022 01:50 SM 2340 B-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 916 Calcium 14.9 0.075 mg/L 0.30 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1045 Iron 680 30 ug/L 120 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 927 Magnesium 3.81 0.040 mg/L 0.16 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 937 Potassium 1.3 0.30 mg/L 1.2 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 929 Sodium 10 0.50 mg/L 2.0 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1082 Strontium 64.3 2.0 ug/L 8.0 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1102 Tin 3.0 U 3.0 ug/L 12 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1152 Titanium 1.0 I 0.75 ug/L 3.0 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1087 Vanadium 2.0 U 2.0 ug/L 8.0 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1092 Zinc 5.7 I 5.0 ug/L 20 06-03-2022 09:45 06-08-2022 01:50 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1105 Aluminum 214 5.0 ug/L 20 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1097 Antimony 0.085 I 0.050 ug/L 0.20 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1002 Arsenic 0.94 0.050 ug/L 0.20 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1007 Barium 42.2 0.20 ug/L 0.80 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1012 Beryllium 0.032 I 0.010 ug/L 0.040 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-06-2022 16:09 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1022 Boron 34.1 2.0 ug/L 8.0 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1027 Cadmium 0.020 U 0.020 ug/L 0.080 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1034 Chromium 0.56 I 0.40 ug/L 1.6 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1037 Cobalt 0.257 0.020 ug/L 0.080 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1042 Copper 0.40 U 0.40 ug/L 0.80 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1051 Lead 0.34 I 0.20 ug/L 0.40 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1055 Manganese 44.7 0.10 ug/L 0.40 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1062 Molybdenum 0.21 I 0.15 ug/L 0.60 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-06-2022 16:09 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1067 Nickel 0.56 I 0.50 ug/L 2.0 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1147 Selenium 0.20 U 0.20 ug/L 0.80 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1077 Silver 0.010 U 0.010 ug/L 0.040 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 LITTLE ST. MARYS @ CR 121A 19010046 19010046 06-01-2022 11:35 2331300 1059 Thallium 0.10 U 0.10 ug/L 0.40 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 21:06 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 46570 Hardness 25.5 0.35 mg/L 1.4 06-08-2022 01:58 SM 2340 B-2011 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 916 Calcium 7.19 0.075 mg/L 0.30 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1045 Iron 950 30 ug/L 120 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 927 Magnesium 1.84 0.040 mg/L 0.16 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 937 Potassium 1.1 I 0.30 mg/L 1.2 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 929 Sodium 6.9 0.50 mg/L 2.0 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1082 Strontium 28.8 2.0 ug/L 8.0 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1102 Tin 3.0 U 3.0 ug/L 12 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1152 Titanium 1.1 I 0.75 ug/L 3.0 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1087 Vanadium 2.0 U 2.0 ug/L 8.0 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1092 Zinc 5.0 U 5.0 ug/L 20 06-03-2022 09:45 06-08-2022 01:58 EPA 200.7 Rev. 4.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1105 Aluminum 330 5.0 ug/L 20 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1097 Antimony 0.054 I 0.050 ug/L 0.20 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1002 Arsenic 0.78 0.050 ug/L 0.20 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1007 Barium 24.2 0.20 ug/L 0.80 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1012 Beryllium 0.030 I 0.010 ug/L 0.040 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-06-2022 16:15 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1022 Boron 23.1 2.0 ug/L 8.0 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1027 Cadmium 0.020 U 0.020 ug/L 0.080 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1034 Chromium 0.58 I 0.40 ug/L 1.6 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1037 Cobalt 0.229 0.020 ug/L 0.080 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1042 Copper 0.40 U 0.40 ug/L 0.80 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1051 Lead 0.46 0.20 ug/L 0.40 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1055 Manganese 30.8 0.10 ug/L 0.40 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1062 Molybdenum 0.15 U 0.15 ug/L 0.60 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1067 Nickel 0.50 U 0.50 ug/L 2.0 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1147 Selenium 0.20 U 0.20 ug/L 0.80 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1077 Silver 0.010 U 0.010 ug/L 0.040 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger RQ-2022-06-06-31 Little St Marys River @ SR 115A 19010032 19010032 06-01-2022 11:05 2331301 1059 Thallium 0.10 U 0.10 ug/L 0.40 Batch matrix spike recoveries for manganese are unavailable for one of two spiked samples because of high analyte concentration in the QC sample. 06-03-2022 09:45 06-03-2022 22:01 EPA 200.8 Rev. 5.4 Jeremy Parrish, Katrin Villinger