RQ-2009-08-03-46 Page 1 of 5 DateofRequest: 29-JUL-2009 SendCoolersTo: CreatedBy:IGOE_AOn:29-JUL-2009 ModifiedBy: BRACKETT_KOn:31-JUL-2009 Phone:850-245-8947 Customer: SIS 2600BlairStoneRoad TwinTowersBldg.MS#4515 Project: SIS-INVEST Tallahassee,FL32399 Division:: Attn:BillMartin District: SamplingEvent: AcreageSamplingPBC SendFinalReportTo: ProgramModuleNumber: 0160 2600BlairStoneRoad Priority: 1 TwinTowersBldg.MS#4515 EventStatus: W CriminalInvestigation: NO Tallahassee,FL32399 ChemistryRequestReviewed BRACKETT_K By: On:31-JUL-2009 Attn:BillMartin BiologyRequestReviewedBy: ReportType: FinalOnly SamplingKitRequired: YESShipon:29-JUL-2009 FTPData: NO SamplingKitShipped: QCReport: YES SamplingKitPackedBy: DateLog: NO DateToReceiveSamples: 03-AUG-2009 Authorization NO Log: ReceivedBy: Comments: PerMikeSole'srequest SuiteA(Water)With60Samples: BottleType:BG-1L NumberofBottles:6 PreservedWith:ICE-NASULF-BISULF W-1-4-DIOX Template:DEFAULT 1,4-DioxaneinAqueousMatricesbyGC/MSusingSIM *1,4-Dioxane BottleType:BG-250ML NumberofBottles:1 PreservedWith:ICE W-AHERB-AA Template:DEFAULT Chlorinated(phenoxyacid)herbicidesinwatermatricesbyHPLC/MS/MS 2,4,5-T 2,4-D Acifluorfen Silvex BottleType:BG-1L NumberofBottles:1 PreservedWith:ICE W-BNA-R Template:DEFAULT EPAMethod8270,Semi-volatileorganicpollutantsincludingPAHs,excludingPCBsandToxaph *Dinoseb *Pentachloroethane 1,2,4,5-Tetrachlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trinitrobenzene 1,3-Dinitrobenzene 1,4-Naphthoquinone 1-Naphthylamine 2,3,4,6-Tetrachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dichlorophenol 2,6-Dinitrotoluene 2-Acetylaminofluorene 2-Chloronaphthalene 2-Chlorophenol 2-Methyl-4,6-dinitrophenol RQ-2009-08-03-46 Page 2 of 5 SuiteA(Water)With60Samples: BottleType:BG-1L NumberofBottles:1 PreservedWith:ICE 2-Methylnaphthalene 2-Naphthylamine 2-Nitroaniline 2-Nitrophenol 2-Picoline 3,3'-Dichlorobenzidine 3,3'-Dimethylbenzidine 3-Methylcholanthrene 3-Nitroaniline 4-Aminobiphenyl 4-Bromophenylphenylether 4-Chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenylphenylether 4-Nitroaniline 4-Nitrophenol 5-Nitro-o-toluidine 7,12-Dimethylbenz(a)anthracene Acenaphthene Acenaphthylene Acetophenone Aniline Anthracene Azobenzene/1,2-Diphenylhydrazine Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzylalcohol Bis(2-chloroethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-ethylhexyl)phthalate Butylbenzylphthalate Chrysene Dibenzo(a,h)anthracene Dibenzofuran Diethylphthalate Dimethylphthalate Dimethylaminoazobenzene Di-n-butylphthalate Di-n-octylphthalate Ethylmethanesulfonate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Hexachloropropene Indeno(1,2,3-cd)pyrene Isophorone Isosafrole m,p-Cresols Methapyrilene Methylmethanesulfonate Naphthalene Nitrobenzene Nitroquinoline-1-oxide N-Nitrosodiethylamine RQ-2009-08-03-46 Page 3 of 5 SuiteA(Water)With60Samples: BottleType:BG-1L NumberofBottles:1 PreservedWith:ICE N-Nitrosodimethylamine N-Nitrosodi-n-propylamine N-Nitrosodiphenylamine/Diphenylamine N-Nitrosomethylethylamine N-Nitrosomorpholine N-Nitrosopiperidine N-Nitrosopyrrolidine o-Cresol o-Toluidine Pentachlorobenzene Pentachloronitrobenzene Pentachlorophenol Phenacetin Phenanthrene Phenol Pyrene Pyridine Safrole BottleType:BG-1L NumberofBottles:1 PreservedWith:ICEAndH2SO4 W-FL-PRO TRPH Template:DEFAULT TotalrecoverablepetroleumhydrocarbonsinwatersamplesbyGC-FID. BottleType:BG-40ML NumberofBottles:1 PreservedWith:ICE W-FUM 1,2-Dibromoethane Template:DEFAULT/50% FumigantsinwatermatricesbyGC/ECD. BottleType:P-1L NumberofBottles:6 PreservedWith:HNO3 W-HG-H-R Mercury Template:DEFAULT MercuryinaqueoussamplesusingcoldvaporAAspectroscopy. W-ICPMS-RTemplate:RCRA/100% TotalRecoverableMetalsanalysisusingICP-MSforaqueoussamplessupportingRCRAProject Arsenic Barium Cadmium Chromium Copper Lead Selenium W-ICP-R Silver Template:NO_TEMPLATE TotalRecoverableMetalsanalysisusingICPemissionspectroscopyforaqueoussamplessuppo Aluminum BottleType:P-125ML NumberofBottles:6 PreservedWith:ICEAndH2SO4 W-NO2NO3 Template:DEFAULT Nitrite/NitrateinaqueousmatricesasmgN/L NO2NO3-N BottleType:BG-1L NumberofBottles:1 PreservedWith:ICE W-PEST-NPTemplate:DEFAULT/100% OrganonitrogenandphosphoruspesticidesinwatermatricesbyGC/NPD. Alachlor Ametryn Atrazine AzinphosMethyl Bromacil Butylate ChlorpyrifosEthyl ChlorpyrifosMethyl Diazinon Ethion Ethoprop Fenamiphos Fonofos Hexazinone Malathion Metalaxyl Metolachlor RQ-2009-08-03-46 Page 4 of 5 SuiteA(Water)With60Samples: BottleType:BG-1L NumberofBottles:1 PreservedWith:ICE Metribuzin Mevinphos Naled Norflurazon ParathionEthyl ParathionMethyl Phorate Prometon Prometryn Simazine W-PSCL-PCB Template:DEFAULT OrganochlorinepesticidesandPCBsinwatermatricesbyGC/ECD. Aldrin Alpha-BHC Beta-BHC Chlordane DDD-p,p' DDE-p,p' DDT-p,p' Delta-BHC Dieldrin EndosulfanI EndosulfanII EndosulfanSulfate Endrin EndrinAldehyde Gamma-BHC Heptachlor HeptachlorEpoxide Methoxychlor PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Toxaphene BottleType:3-G-40MLACIDIF NumberofBottles:6 PreservedWith:IceandHCl W-VOC-A-RTemplate:DFLT-RCRA VolatileorganicpollutantsinacidpreservedwatermatricesusingGC/MS 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2-Butanone Benzene Bromodichloromethane Bromoform Bromomethane Carbontetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane RQ-2009-08-03-46 Page 5 of 5 SuiteA(Water)With60Samples: BottleType:3-G-40MLACIDIF NumberofBottles:6 PreservedWith:IceandHCl Ethylbenzene m,p-Xylene Methylenechloride Methyl-t-butylether o-Xylene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinylchloride SuiteB(Water)With50Samples: BottleType:P-1L NumberofBottles:5 PreservedWith:HNO3 OV-ALPHA Template:DEFAULT GrossAlphainwaterbyoverflowlab Alpha,Total Alpha-CountingError SuiteC(Water)With10Samples: BottleType:P-1L NumberofBottles:2 PreservedWith:HNO3 OV-RADIUMTemplate:DEFAULT Radium226(903.1)and228(Ra-05)byoverflowlab Radium226 Radium226-CountingError Radium228 Radium228-CountingError *-ThelaboratoryisnotNELAPcertifiedforthisanalyte/method,orcertificationisnotapplicable.